Skip to main content
Log in

Interfacing between supercritical fluid chromatography and infrared spectroscopy — A review

  • Review Paper
  • Published:
Chromatographia Aims and scope Submit manuscript

Summary

Coupling of supercritical fluid chromatography (SFC) and infrared spectroscopy (IR) is growing in popularity. SFC/IR is one of the important hyphenated techniques in modern analytical chemistry. Basically two types of interfacing approaches have been introduced: direct flow cell and solvent elimination. These techniques are reviewed and their advantages and disadvantages are discussed.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. E. Klesper, A. H. Corwin, D. A. Turner, J. Org. Chem.,27, 700 (1962).

    CAS  Google Scholar 

  2. M. N. Myers, J. C. Giddings, Sep. Sci.,1, 761 (1966).

    CAS  Google Scholar 

  3. L. McLaren, M. N. Myers, J. C. Giddings, Science,159, 197 (1968).

    CAS  Google Scholar 

  4. J. C. Giddings, M. N. Myers, J. W. King, J. Chromatogr. Sci.,7, 276 (1969).

    CAS  Google Scholar 

  5. S. T. Sie, G. W. A. Rijnders, Sep. Sci.,2, 699 (1967).

    CAS  Google Scholar 

  6. S. T. Sie, G. W. A. Rijnders, Sep. Sci.,2, 729 (1967).

    CAS  Google Scholar 

  7. S. T. Sie, G. W. A. Rijnders, Sep. Sci.,2, 755 (1967).

    CAS  Google Scholar 

  8. S. T. Sie, W. Van Beersum, G. W. A. Rijnders, Sep. Sci.,1, 459 (1966).

    CAS  Google Scholar 

  9. L. G. Randall, inS. Ahuja (Editor), Ultrahigh Resolution Chromatography, ASC Symposium Series No. 250, American Chemical Society, Washington, D. C., 1984, pp. 135–169.

    Google Scholar 

  10. W. P. Jackson, B. E. Richter, J. C. Fjeldsted, R. C. Kong, M. L. Lee, inS. Ahuja (Editor), Ultrahigh Resolution Chromatography, ACS Symposium Series No. 250, American Chemical Society, Washington, D. C., 1984, pp. 121–133.

    Google Scholar 

  11. E. Klesper, Angew. Chem. Int. Ed. Engl.,17, 738 (1978).

    Article  Google Scholar 

  12. U. van Wasen, I. Swaid, G. M. Schreider, Angew. Chem. Int. Ed. Engl.,19, 575 (1980).

    Google Scholar 

  13. T. H. Gouw, R. E. Jentoft, J. Chromatogr.68, 303 (1972).

    Article  CAS  Google Scholar 

  14. T. H. Gouw, R. E. Jentoft, inJ. C. Giddings, Y. H. Yoon, K. D. Caldwell, M. N. Myers andM. E. Howingh (Editors), Advances in Chromatography, Volume 13, Marcel Dekker, New York, 1975, pp. 1–40.

    Google Scholar 

  15. P. A. Peaden, M. L. Lee, J. Liq. Chromatogr.,5, 179 (1982).

    CAS  Google Scholar 

  16. L. G. Randall, Sep. Sci. Technol.,17, 1 (1982).

    CAS  Google Scholar 

  17. E. Klesper, W. Hartmann, Eur. Polym. J.,14, 77 (1978).

    CAS  Google Scholar 

  18. M. Novotny, S. R. Springston, P. A. Peaden, J. C. Fjeldsted, M. L. Lee, Anal. Chem.,53, 407A (1981).

    CAS  Google Scholar 

  19. Special Issue for SFC. J. High Resolu. Chromatogr./Chromatogr. Commun.,9, March Issue (1986).

  20. Special Issue for SFC, J. Chromatogr. Sci.,24, June Issue (1986).

  21. M. N. Myers, J. C. Giddings, inE. S. Perry andC. J. Van Oss (Editors), Progress in Separation and Purification, Vol. 3, Wiley-Interscience, New York, 1970, pp. 133–152.

    Google Scholar 

  22. D. Bartmann, Ber. Bunsenges. Phys. Chem.,76, 336 (1972).

    CAS  Google Scholar 

  23. J. C. Fjeldsted, R. C. Kong, M. L. Lee, J. Chromatogr.,279, 449 (1983).

    CAS  Google Scholar 

  24. P. A. Peaden, J. C. Fjeldsted, M. L. Lee, S. R. Springston, M. Novotny, Anal. Chem.54, 1090 (1982).

    CAS  Google Scholar 

  25. J. C. Fjeldsted, B. E. Richter, W. P. Jackson, M. L. Lee, J. Chromatogr.,279, 423 (1983).

    CAS  Google Scholar 

  26. W. Asche, Chromatographia,11, 411 (1978).

    Article  CAS  Google Scholar 

  27. R. D. Smith, W. D. Felix, J. C. Fjeldsted, M. L. Lee, Anal. Chem.,54, 1883 (1982).

    CAS  Google Scholar 

  28. J. Henion, inP. Kucera (Editor), Microcolumn High-Performance Liquid Chromatography, Elsevier, Amsterdam, 1984, pp. 260–300.

    Google Scholar 

  29. R. D. Smith, J. C. Fjeldsted, M. L. Lee, J. Chromatogr.,247, 231 (1982).

    Article  CAS  Google Scholar 

  30. R. D. Smith, H. R. Udseth, Anal. Chem.,55, 2476 (1983).

    Google Scholar 

  31. R. D. Smith, H. R. Udseth, H. T. Kalinoski, Anal. Chem.,56, 2971 (1984).

    CAS  Google Scholar 

  32. B. W. Wright, H. T. Kalinoski, R. D. Smith, Anal. Chem.,58, 2823 (1985).

    Google Scholar 

  33. R. D. Smith, B. W. Wright, H. R. Udseth, inS. Ahuja (Editor), Chromatography and Separation Chemistry-Advances and Developments, ACS Symposium Series No. 297, American Chemical Society, Washington, D. C., 1986, pp. 260–293.

    Google Scholar 

  34. R. D. Smith, H. R. Udseth, Biomed. Mass Spectrom.,10, 577 (1983).

    CAS  Google Scholar 

  35. R. D. Smith, H. R. Udseth, B. W. Wright, J. Chromatogr. Sci.,23, 192 (1985).

    CAS  Google Scholar 

  36. R. D. Smith, B. W. Wright, H. R. Udeth, inJ. G. Nikely (Editor), Advances in Capillary Chromatography, Huethig, Heidelberg, 1985, pp. 56–94.

    Google Scholar 

  37. R. D. Smith, H. R. Udseth, Sep. Sci. Techn.,18, 245 (1983).

    CAS  Google Scholar 

  38. K. Jinno, inE. S. Yeung (Editor), Detectors in Liquid Chromatography, Wiley-Interscience, New York, 1986, in press.

    Google Scholar 

  39. K. Shafer, P. R. Griffiths, Anal. Chem.,55, 1939 (1983).

    Article  CAS  Google Scholar 

  40. S. V. Olesik, S. B. French, M. Novotny, Chromatographia,18, 489 (1984).

    Article  CAS  Google Scholar 

  41. C. C. Johnson, J. W. Jordan, L. T. Taylor, D. W. Vidrine, Chromatographia,20, 717 (1985).

    Article  CAS  Google Scholar 

  42. M. E. Hughes, J. L. Fasching, J. Chromatogr. Sci.,24, 535 (1985).

    Google Scholar 

  43. G. Herzberg, Infrared and Raman Spectra of Polyatomic Molecules, Van Nostrand, New York, 1949.

    Google Scholar 

  44. J. A. deHaseth, T. L. Isenhour, Anal. Chem.,49, 1977 (1977).

    CAS  Google Scholar 

  45. J. W. Jordan, L. T. Taylor, J. Chromatogr. Sci.,24, 82 (1986).

    CAS  Google Scholar 

  46. J. W. Hellgeth, J. W. Jordan, L. T. Taylor, M. Ashraf Khorassani, J. Chromatogr. Sci.,24, 183 (1986).

    CAS  Google Scholar 

  47. P. M. Rentzepis, D. C. Douglas, Nature (London),293, 165 (1981).

    Article  CAS  Google Scholar 

  48. S. B. French, M. Novotny, Anal. Chem.,58, 164 (1986).

    Article  CAS  Google Scholar 

  49. K. Jinno, C. Fujimoto, T. Takeuchi, M. Ideriha, D. Ishii, Bunseki Kagaku (Japanese),29, 612 (1980).

    CAS  Google Scholar 

  50. K. Jinno, C. Fujimoto, J. High Resolut. Chromatogr./Chromatogr. Commun.,4, 532 (1981).

    CAS  Google Scholar 

  51. K. Jinno, Spectrosc. Lett.,14, 659 (1981).

    CAS  Google Scholar 

  52. K. Jinno, C. Fujimoto, Y. Hirata, Appl. Spectrosc.,36, 67 (1982).

    Article  CAS  Google Scholar 

  53. K. Jinno, C. Fujimoto, D. Ishii J. Chromatogr.,239, 625 (1982).

    CAS  Google Scholar 

  54. C. Fujimoto, K. Jinno, Y. Hirata, J. Chromatogr.,258, 81 (1983).

    Article  CAS  Google Scholar 

  55. C. Fujimoto, T. Oosuka, K. Jinno, Anal. Chim. Acta,178, 159 (1985).

    Article  CAS  Google Scholar 

  56. D. Kuehl, P. R. Griffiths, J. Chromatogr. Sci.,17, 471 (1979).

    CAS  Google Scholar 

  57. D. Kuehl, P. R. Griffiths, Anal. Chem.,52, 1394 (1980).

    CAS  Google Scholar 

  58. C. M. Conroy, P. R. Griffiths, K. Jinno, Anal. Chem.,57, 822 (1985).

    Article  CAS  Google Scholar 

  59. C. M. Conroy, P. R. Griffiths, P. J. Duff, L. V. Azarraga, Anal. Chem.,56, 2636 (1984).

    Article  CAS  Google Scholar 

  60. K. S. Kalasinsky, J. T. McDonald, Jr., V. F. Kalasinsky, inJ. Christensen (Editor), FT-IR Spectral Lines, Vol. 5, Nicholet Instrument Corp., Madison, 1983, p. 14.

    Google Scholar 

  61. K. S. Kalasinsky, J. A. Smith, V. F. Kalasinsky, Anal. Chem.,57 1969 (1985).

    Article  CAS  Google Scholar 

  62. K. H. Shafer, S. L. Pentony, Jr., P. R. Griffiths, J. High Resolut. Chromatogr./Chromatogr. Commun.,7, 707 (1984).

    Article  CAS  Google Scholar 

  63. K. H. Shafer, S. L. Pentony, Jr., P. R. Griffiths, Anal. Chem.,58, 58 (1986).

    CAS  Google Scholar 

  64. S. L. Pentony, Jr., K. H. Shafer, P. R. Griffiths, R. Fucuo, J. High Resolut. Chromatogr./Chromatogr. Commun.,9, 168 (1986).

    Google Scholar 

  65. S. L. Pentony, Jr., K. H. Shafer, P. R. Griffiths, J. Chromatogr. Sci.,24, 230 (1986).

    Google Scholar 

  66. C. Fujimoto, Y. Hirata, K. Jinno, J. Chromatogr.,332, 47 (1985).

    Article  CAS  Google Scholar 

  67. P. R. Griffiths, Chemical Infrared Fourier Transform Spectroscopy, Wiley-Interscience, New York, 1975.

    Google Scholar 

  68. K. Jinno, C. Fujimoto, Y. Hirata, D. Ishii, inM. Novotny andD. Ishii (Editors). Microcolumn Separations, Elsevier, Amsterdam, 1985, pp. 177–196.

    Google Scholar 

  69. K. Jinno, JEOL News (in Japanese)23, 2 (1983).

    Google Scholar 

  70. P. R. Griffiths, J. A. deHaseth, Fourier Transform Infrared Spectrometry, Wiley-Interscience, New York, 1986.

    Google Scholar 

  71. J. A. Nieman, L. B. Rogers, Sep. Sci.,10, 517 (1975).

    CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Jinno, K. Interfacing between supercritical fluid chromatography and infrared spectroscopy — A review. Chromatographia 23, 55–62 (1987). https://doi.org/10.1007/BF02310421

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02310421

Key Words

Navigation