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Validation of an HPLC method for the determination of *-dichlorobenzene and naphthalene in mothrepellents

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Abstract

 The determination of dichlorobenzene and naphthalene in commercial repellents used in Spain has been validated. This was done using an isocratic regime, to test the reverse -phase HPLC system with acetonitrile: water 65 : 35 (v: v) as the mobile phase, at 20  °C. This technique is proposed for the modular validation of the HPLC system . The results obtained with this method show good agreement with the results provided by the manufacturers of the mothrepellents.

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Authors and Affiliations

  1. University of Zaragoza, Analytical Chemistry Department. Crtra. Zaragoza, s/n, 22071 Huesca, Spain. e-mail: cdiaz@posta.unizar.es Tel.: +34-9-74 239320 Fax: +34-9-74 239302, , , , , , ES

    R. C. Díaz, M. A. Sarasa, C. Ríos & J. J. Cuello

Authors
  1. R. C. Díaz
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  2. M. A. Sarasa
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  3. C. Ríos
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  4. J. J. Cuello
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Received: 21 December 1998 / Accepted: 4 May 1999

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Díaz, R., Sarasa, M., Ríos, C. et al. Validation of an HPLC method for the determination of *-dichlorobenzene and naphthalene in mothrepellents. Accred Qual Assur 4, 473–476 (1999). https://doi.org/10.1007/s007690050414

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  • DOI: https://doi.org/10.1007/s007690050414

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