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Synthesis of vinyloxy phosphorus monomers from the enolate of acetaldehyde

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Summary

A simple synthetic procedure for vinyloxy phosphorus monomers involves the reaction of the enolate of acetaldehyde, obtained from the cycloreversion of tetrahydrofuran in the presence of n-butyllithium, with chlorophosphites or phosphorochloridates leading to vinyl phosphites or vinyl phosphates, respectively, in high yield and purity.

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Authors and Affiliations

  1. Carl S. Marvel Laboratories, Department of Chemistry, The University of Arizona, Tucson AZ 85721-0041, , , , , , XX

    K. F. Johnston, Anne Buyle Padias & H. K. Hall

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  1. K. F. Johnston
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  2. Anne Buyle Padias
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  3. H. K. Hall
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Additional information

Received: 17 August 2000/Accepted: 8 September 2000

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Johnston, K., Padias, A. & Hall, H. Synthesis of vinyloxy phosphorus monomers from the enolate of acetaldehyde. Polymer Bulletin 45, 359–364 (2000). https://doi.org/10.1007/s002890070008

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  • DOI: https://doi.org/10.1007/s002890070008

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