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Coulometric titrations with an ion exchange separation step

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Summary

The coupling is described of coulometric separation methods with an ion exchange separation step. Various methods of enrichment and separation are described using the analysis of nitrogen compounds, such as ammonia, urea and nitrite, as examples. A microcomputer controls the separation step and regulates the coulometric determination. Quantitative separations are achieved in all cases, so that the advantage of coulometric titration, as a precise absolute determination method, is retained.

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References

  1. Rüttinger HH, Spohn U (1987) Anal Chim Acta 202:75

    Google Scholar 

  2. Spohn U, Hahn M, Rüttinger HH, Matschiner H (1989) Fresenius Z Anal Chem 333:39

    Google Scholar 

  3. Spohn U, Hahn M, Rüttinger HH, Matschiner H (1989) Galvanotechnik 80:973

    Google Scholar 

  4. Matschiner H, Rüttinger HH (1987) Feingerätetechnik 36:170

    Google Scholar 

  5. Hahn M, Schiede H (1988) unveröffentlichte Ergebnisse

  6. Hahn M, Rüttinger HH, Matschiner H, Lenk N (1991) Fresenius J Anal Chem 340:22

    Google Scholar 

  7. Spohn U, Hahn M, Matschiner H, Ehlers G, Berge H (1989) Fresenius Z Anal Chem 332:849

    Google Scholar 

  8. Hahn M, Rüttinger HH, Matschiner H (1992) Fresenius J Anal Chem 343:269

    Google Scholar 

  9. Hoffman HJ, Röhl (1985) LaborPraxis 9:330

    Google Scholar 

  10. Schnitzler M (1986) LaborPraxis 10:214

    Google Scholar 

  11. Essing A, Umland F (1989) Fresenius Z Anal Chem 335:826

    Google Scholar 

  12. Sontheimer H, Schnitzler M (1982) Vom Wasser 59:169

    Google Scholar 

  13. Hahn M, Rüttinger HH, Matschiner H (1991) Z Wasser-Abwasser-Forsch 24:191

    Google Scholar 

  14. Essing A, Umland F (1986) Fresenius Z Anal Chem 325:8

    Google Scholar 

  15. Bidlo Z, Berger T, Gruntz U (1989) Vom Wasser 73:1

    Google Scholar 

  16. Hahn M, Rüttinger HH, Matschiner H (1991) Z Wasser-Abwasser-Forsch 24:188

    Google Scholar 

  17. Weiß J (1991) Ionenchromatographie. VCH, Weinheim New York Basel Cambridge

    Google Scholar 

  18. Haddad PR, Jackson PE (1990) Ion chromatography. J Chromatogr lib. vol. 46. Elsevier, Amsterdam Oxford New York Tokyo

    Google Scholar 

  19. Fang Z, Ruzicka J, Hansen EH (1984) Anal Chim Acta 164:23

    Google Scholar 

  20. Fang Z, Xu S, Zhang S (1984) Anal Chim Acta 164:41

    Google Scholar 

  21. Hirata S, Honda K, Kumamaru T (1989) Anal Chim Acta 221:65

    Google Scholar 

  22. Ruzicka J, Hansen EH (1988) Flow injection analysis. Wiley, New York

    Google Scholar 

  23. Valcarcel M, Luque de Castro MD (1987) J Chromatogr 393:3

    Google Scholar 

  24. Luque de Castro MD (1989) Talanta 36:591

    Google Scholar 

  25. Faizullah AT, Townshend A (1986) Anal Chim Acta 179:233

    Google Scholar 

  26. Bergamin FH, Reis BF, Jacintho AO, Zagatto EAG (1980) Anal Chim Acta 117:81

    Google Scholar 

  27. Schulze G, Liu CY, Brodowski M, Elsholz O, Frenzel W, Moeller J (1988) Anal Chim Acta 214:121

    Google Scholar 

  28. Fang Z, Zhu Z, Zhang S, Xu S, Guo L, Sun L (1988) Anal Chim Acta 214:41

    Google Scholar 

  29. Sohrin Y, Isshiki K, Nakayama E, Kihara S, Matsui M (1989) Anal Chim Acta 218:25

    Google Scholar 

  30. Schulze G, Elsholz O (1989) Fresenius Z Anal Chem 335:721

    Google Scholar 

  31. Karlsson M, Persson JA, Moeller J (1991) Anal Chim Acta 244:109

    Google Scholar 

  32. Hajos P, Inczedy J (1980) J Chromatogr 201:193

    Google Scholar 

  33. Barikov VG, Songina OA, Sereda TG (1972) Zavodsk Lab 38:641

    Google Scholar 

  34. Krivis AF, Supp GR, Gaza FS (1963) Anal Chem 35:2216

    Google Scholar 

  35. Spohn U (1987) Dissertation, Universität Halle

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Authors and Affiliations

  1. Institut für Analytische Chemie, Fachbereich Chemie der Martin-Luther-Universität, Weinbergweg 16, O-4020, Halle S., Federal Republic of Germany

    M. Hahn, C. Voigt, H. H. Rüttinger & H. Matschiner

Authors
  1. M. Hahn
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  2. C. Voigt
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  3. H. H. Rüttinger
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  4. H. Matschiner
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Hahn, M., Voigt, C., Rüttinger, H.H. et al. Coulometric titrations with an ion exchange separation step. Fresenius J Anal Chem 344, 311–315 (1992). https://doi.org/10.1007/BF00321838

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  • DOI: https://doi.org/10.1007/BF00321838

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