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Structure of substituted aminomethanebisphosphonic acids analyzed by NMR spectroscopy and X-ray powder diffraction

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  • Spectrometric Investigations
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Abstract

The 31P NMR spectra of a series of substituted aminomethanebisphosphonic acids (AMBAs) are reported. The AMBAs may crystallize as anhydrates or in hydrated form. The appearance of more than one 31P NMR signal in the solid state NMR spectra of AMBAs is an indication for a complex molecular order with non-equivalent phosphorus sites.

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Authors and Affiliations

  1. Federal Institute for Materials Research and Testing (BAM), D-12489, Berlin, Germany

    H. Jancke

  2. Institute for Applied Chemistry Adlershof, D-12484, Berlin, Germany

    B. Costisella & K. Jancke

Authors
  1. H. Jancke
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  2. B. Costisella
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  3. K. Jancke
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Dedicated to Professor Dr. H. Kriegsmann on the occasion of his 70th birthday

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Jancke, H., Costisella, B. & Jancke, K. Structure of substituted aminomethanebisphosphonic acids analyzed by NMR spectroscopy and X-ray powder diffraction. Fresenius J Anal Chem 352, 496–498 (1995). https://doi.org/10.1007/BF00323374

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  • DOI: https://doi.org/10.1007/BF00323374

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