Skip to main content
SpringerLink
Log in

The crystal structure of 2-benzoylpyridine N4-methyl-N4-phenylthiosemicarbazone

  • Note
  • Published:
Journal of Chemical Crystallography Aims and scope Submit manuscript

Abstract

2-Benzoylpyridine N4-methyl-N4-phenylthiosemicarbazone, HBz4MePh, monoclinic,P2(1)/n a=9.141(2),b=18.507(4),c=11.401(2) Å, β=110.58(3)o,V=1805.6(9) Å3,Z=4, μ=1.655 mm−1. HBz4MePh crystallizes in a hydrogen bonded Z isomeric conformation with respect to the C7−N2 bond. The intramolecular hydrogen bond is between N3−H...N1, and the S atom isZ to the azomethine nitrogne, N2.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Liberta, A.E.; West, D.X.BioMetals 1992,5, 121.

    Google Scholar 

  2. West, D.X.; Mokijewski, B.L.; Gebremedhin, H.; Romack, T.J.Transition Met. Chem. 1992,17, 384–386.

    Google Scholar 

  3. Palenik, G.J.; Rendle, D.F.; Carter W.S.Acta Crystallogr. 1974,B30, 2390.

    Google Scholar 

  4. West, D.X.; Bain, G.A.; Butcher, R.J.; Jasinski, J.P.; Li, Y.; Pozdniakiv, R.Y.; Valdés-Martínez, J.; Toscano, R.A.; Hernández-Ortega, S.Polyhedron 1996,15, 665.

    Google Scholar 

  5. Korp, J.D.; Bernal, I.; Lemke, T.L.J. Heterocyclic Chem. 1977,14, 709.

    Google Scholar 

  6. West, D.X.; Ahrweiler, P.M.; Ertem, G.; Scovill, J.P.; Klayman, D.L. Flippen-Anderson, J.L.; Gilardi, R.; George, C.; Pannell, L.K.Transition Met. Chem. 1985,10, 264.

    Google Scholar 

  7. West, D.X.; Ives, J.S.; Krejci, J.; Salberg, M.M.; Zumbhalen, T.L.; Bain, G.A.; Liberta, A.E.; Valdés-Martínez J.; Hernández-Ortega, S.; Toscano, R.A.Polyhedron 1995,14, 2189.

    Google Scholar 

  8. Scovill, J.P.Phosph. Sulf. Sil. 1991,60, 15.

    Google Scholar 

  9. West, D.X.; Padhye S.B.; Sonawane, P.B.Struct. Bond. 1991,76, 1.

    Google Scholar 

  10. West, D.X.; Kozub, N.M.; Bain, G.A.Transition Met. Chem. 1996,21, 52.

    Google Scholar 

  11. West, D.X.; Salberg, M.M.; Bain, G.A.; Liberta, A.E.; Valdés-Martínez, J.; Hernández-Ortega, S.Transition Met. Chem. 1996,21, 206.

    Google Scholar 

  12. West, D.X.; Yang, Y-H.; Klein, T.L.; Goldberg, K.I.; Liberta, A.E.; Valdés-Martínez, J.; Toscano, R.A.Polyhedron 1995,14, 1681.

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Instituto de Química, Universidad Nacional Autónoma de México, Circuito Exterior, Ciudad Universitaria, Coyoacán, 04510, México, D.F.

    Jesús Valdés-Martínez & Simon Hernández-Ortega

  2. Department of Chemistry, Illinois State University, 61790-4160, Normal, Illinois

    Douglas X. West, Amy M. Stark & Gordon A. Bain

Authors
  1. Jesús Valdés-Martínez
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Simon Hernández-Ortega
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Douglas X. West
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Amy M. Stark
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. Gordon A. Bain
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Valdés-Martínez, J., Hernández-Ortega, S., West, D.X. et al. The crystal structure of 2-benzoylpyridine N4-methyl-N4-phenylthiosemicarbazone. J Chem Crystallogr 26, 861–864 (1996). https://doi.org/10.1007/BF01670320

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01670320

Key Words

Search

Navigation