Abstract
The high temperature superconductors of the system Bi-Pb-Sr-Ca-Cu-O show promising properties and large scale applications can be considered. The (Bi,Pb)2Sr2Ca2Cu3O10+δ (Bi,Pb(2223)) phase is attractive because of its high superconducting temperature (110 K) and high current transport capabilities.
Simultaneous DTA/TG has proved an excellent tool for synthesizing, characterizing these high temperature superconductors, confirming phase diagrams and finding the optimal annealing temperature for Bi,Pb(2223)/Ag tapes in order to obtain high critical current densities around 30 kA cm−2 at 77 K and 0T. The identification of the main DTA peaks of measurement of different phase mixtures made it possible to observe the formation of an intermediate phase Bi,Pb(2212) during the formation of Bi,Pb(2223).
Similar content being viewed by others
References
H. Maeda, Y. Tanaka, M. Fukutomi and T. Asano, Japanese J. Appl. Phys., 27 (1988) L209.
K. Schulze, P. Majewski, B. Hettich and G. Petzow, Zeit. Metallkunde, 81 (1990) 836.
U. Endo, S. Koyama and T. Kawai, Japanese J. Appl. Phys., 27 (1988) L1476.
S. Koyama, U. Endo and T. Kawai, Japanese J. Appl. Phys., 27 (1988) L1861.
M. Takano, I Takada, K. Oda, H. Kitaguchi, Y. Miura, Y. Ikeda, Y. Tomii and H. Mazaki, Japanese J. Appl. Phys., 27 (1988) L1041.
G. Grasso, A. Jeremie and R. Flükiger, Superconductor Sci. Technol., 8 (1995) 827; and G. Grasso, B. Hensel, A. Jeremie and R. Flükiger, Physica, C 241 (1995) 45.
A. M. M. Gadalla and J. White, Trans. British Ceram. Soc., 65 (1966) 181.
R. S. Roth, C. J. Rawn, J. J. Ritter and B. P. Burton, J. Amer. Ceram. Soc., 72 (1989) 1545.
A. Jeremie, Ph.D. Thesis, University of Geneva 1995, p. 2762.
H. Kitaguchi, J. Takada, K. Oda and Y. Miura, J. Mater. Res., 5 (1990) 929.
U. Kuxmann and P. Fischer, Erzmetall, 27 (1974) 533.
H. Assmann, A. Günther, K. Rigby and M. Wohlfart, Advances in Superconductivity V, Edts Y. Bando and H. Yamauchi, Tokyo, Japan 1993 p. 685.
R. Flükiger, B. Hensel, A. Pollini, J.-C. Grivel, A. Perin and A. Jeremie, Proceedings of ISS92, Kobe, Japan, November 1992, p. 17.
A. Jeremie, J.-C. Grivel and R. Flükiger, Physica C, 235-240 (1994) 943.
T. G. Holesinger, D. J. Miller and L. S. Chumbley, Physica C, 217 (1993) 85.
R. Flükiger, G. Grasso, B. Hensel, M. Daumling, R. Gladyshevsku, A. Jeremie, J.-C. Grivel and A. Perin in “Bismuth-based High Temperature Superconductors” Eds. H. Maeda and K.Togano, to be published.
Y. Iwai, Y. Hoshi, H. Saito and M. Takata, Physica C, 170 (1990) 319.
M. Schlichenmaier and S. Kemmler-Sack, Physica C, 198 (1992) 175.
A. Jeremie, K. Alami-Yadri, J.-C. Grivel and R. Flükiger, Superconductor Sci. Technol., 6 (1993) 730.
K. Aota, H. Hattori, T. Hatano, K. Nakamura and K. Ogawa, Japanese J. Appl. Phys., 28 (1989) L2196.
“CRC Handbook of Chemistry and Physics 1913–1995”, 75th Edition, David R. Lide, Editor-in-Chief, CRC Press Inc. 1994, p. 4–36.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Jeremie, A., Grasso, G. & Flükiger, R. Synthesis and characterization of high temperature superconductors. Journal of Thermal Analysis 48, 635–645 (1997). https://doi.org/10.1007/BF01979509
Issue Date:
DOI: https://doi.org/10.1007/BF01979509