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Use of Eu(DPM)3 to study the long-range spin-spin coupling of1H-1H and1H-14N via the PMR spectra

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

Employing heteronuclear double resonance and paramagnetic additives it was established that the additional broadening of the signals in the PMR spectrum of 1-vinylimidazole is caused by the1H -14N spin-spin coupling, while in the spectrum of 1-vinylpyrazole it is caused, in addition, by the long-range1H-1H spin -spin coupling via six bonds.

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Literature cited

  1. V. K. Voronov, Izv. Sibirsk. Otd. Akad. Nauk SSSR, Ser. Khim. Nauk, 67 (1971).

  2. M. Witanowski, L. Stefanik, H. Stefanik, H. Januszewski, and Z. W. Wolkowski, Chem. Commun., 1573 (1971).

  3. M. Hirayama, E. Edagawa, and Y. Hanyu, Chem. Commun., 1343 (1972).

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Authors and Affiliations

  1. Irkutsk Institute of Organic Chemistry, Siberian Branch of the Academy of Sciences of the USSR, USSR

    V. K. Voronov, V. I. Glukhikh, E. S. Domnina & G. G. Skvortsova

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  1. V. K. Voronov
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  2. V. I. Glukhikh
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  3. E. S. Domnina
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  4. G. G. Skvortsova
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 1, pp. 200–201, January, 1977.

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Voronov, V.K., Glukhikh, V.I., Domnina, E.S. et al. Use of Eu(DPM)3 to study the long-range spin-spin coupling of1H-1H and1H-14N via the PMR spectra. Russ Chem Bull 26, 176–177 (1977). https://doi.org/10.1007/BF00921524

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  • DOI: https://doi.org/10.1007/BF00921524

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