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Tetracyclines Communication 33. Synthesis of 8-chloro-5-methoxy-3,10-dioxo-1,2,3,4,4a,9,9a,10-octahydroanthracene [5-chloro-1,3,4,4a,9a,10-hexahydro-8-methoxy-2,9-anthracenedione]

  • Organic and Biological Chemistry
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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Summary

8-Chloro-5-methoxy-3,10-dioxo-1,2,3,4,4aβ,9,9aα,10-octahydroanthracene (Ib) was synthesized; this can serve as an intermediary in the preparation of the tetracyclic analog (IIb) of aureomycin,

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Literature cited

  1. I. G. Bolesov, M. N. Kolosov, and M. M. Shemyakin, Dokl. AN SSSR,151, 1097 (1963).

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  2. Yu. A. Arbuzov, I. Bregadze, M. N. Kolosov, I. G. Bolesov, M. M. Shemyakin, and E. A. Él'perina, Izv. AN SSSR. Ser. khim.,1964, 310.

  3. H. E. Faith, M. E. Bahler, and H. J. Florestano, J. Amer. dem. Soc.,77, 546 (1955).

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Authors and Affiliations

  1. Institute for the Chemistry of Natural Products, Academy of Sciences, USSR

    Yu. A. Arbuzov, I. G. Bolesov, A. L. Zhuze, M. N. Kolosov, L. K. Osanova & M. M. Shemyakin

Authors
  1. Yu. A. Arbuzov
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  2. I. G. Bolesov
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  3. A. L. Zhuze
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  4. M. N. Kolosov
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  5. L. K. Osanova
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  6. M. M. Shemyakin
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 5, pp. 806–810, May, 1965 Original article submitted April 22, 1963

For preceding communication see [1],

The authors thank L. B. Senyavina for infrared spectrum measurements.

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Arbuzov, Y.A., Bolesov, I.G., Zhuze, A.L. et al. Tetracyclines Communication 33. Synthesis of 8-chloro-5-methoxy-3,10-dioxo-1,2,3,4,4a,9,9a,10-octahydroanthracene [5-chloro-1,3,4,4a,9a,10-hexahydro-8-methoxy-2,9-anthracenedione]. Russ Chem Bull 14, 786–789 (1965). https://doi.org/10.1007/BF00845688

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  • DOI: https://doi.org/10.1007/BF00845688

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