Skip to main content
SpringerLink
Log in

Separation of polycyclic aromatic hydrocarbons under isocratic conditions by a column switching technique

  • Originals
  • Published:
Chromatographia Aims and scope Submit manuscript

Summary

A simple and efficient method of separating a 20-component PAH-mixture (RSM 1647 standard mixture +benzene, toluene, perylene and coronene) by RP-HPLC is described. Separation was by using two Superspher-100 RP-18 cartridges thermostatted at different temperatures under isocratic conditions with water-acetonitrile eluent. The analysis time with complete resolution of all components can be reduced to 15 min.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. K. G. Liphard, GIT Fachz. Lab.4, 323 (1992).

    Google Scholar 

  2. I. Lamprecht, J. F. K. Huber, Chromatographia34, 376 (1992).

    Google Scholar 

  3. I. Schmit, R. A. Henry, R. C. Williams, J. F. Dieckman, J. Chromatogr. Sci.9, 645 (1971).

    Google Scholar 

  4. Fed. Regist., 44 (No. 233), 69514 (1979).

  5. C. Sander, S. A. Wise, Adv. Chrom.25, 139 (1986).

    Google Scholar 

  6. C. Sander, S. A. Wise, CRC Crit. Rev. Anal. Chem.18, 299 (1988).

    Google Scholar 

  7. C. Sander, S. A. Wise, J. Chromatogr.316, 163 (1989).

    Google Scholar 

  8. M. Stalcup, D. E. Martire, S. A. Wise, J. Chromatogr.442, 1 (1988).

    Google Scholar 

  9. C. Sander, S. A. Wise, Anal. Chem.61, 1749 (1989).

    Google Scholar 

  10. W. Chmielowiec, H. Sawatzky, J. Chromatogr. Sci.17, 245 (1979).

    Google Scholar 

  11. J. F. K. Huber, R. van der Linden, E. Ecker, M. Oreans, J. Chromatogr.83, 267 (1973).

    Google Scholar 

  12. F. Eisenbeiß, S. Ehlerding, Kontakte1, 22 (1978).

    Google Scholar 

  13. J. F. K. Huber, F. Eisenbeiß, J. Chromatogr.149, 127 (1978).

    Google Scholar 

  14. Chromatographie-Katalog Merck, 1989, p. 44.

  15. C. Sander, S. A. Wise, J. H. R. C. & C. C.11, 383 (1988).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Institut für Anorganische Chemie und Analytische Chemie, J. Gutenberg Universität, 55099, Mainz, Germany

    A. Kurganov & K. K. Unger

  2. R & D. Chromatography, E. Merck, 64271, Darmstadt, Germany

    F. Eisenbeiß

Authors
  1. A. Kurganov
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. K. K. Unger
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. F. Eisenbeiß
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Kurganov, A., Unger, K.K. & Eisenbeiß, F. Separation of polycyclic aromatic hydrocarbons under isocratic conditions by a column switching technique. Chromatographia 39, 175–179 (1994). https://doi.org/10.1007/BF02274497

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02274497

Key Words

Search

Navigation