Summary
This paper describes the gas chromatographic separation of the mixture of di- and mono-O-isopropylidene-D-glucose and D-glucose as their trimethylsilyl derivatives. The use of OV-101 as liquid phase provides a complete separation for the all components in the mixture. Quantative analysis was performed using xylitol as the internal standard for di- and mono-O-isopropylidene-D-glucose, and sorbitol as the internal standard for α-and β-glucose.
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Novina, R. Gas-liquid chromatography of isopropylidene-glucose and glucose as their trimethylsilyl derivatives. Chromatographia 18, 21–22 (1984). https://doi.org/10.1007/BF02279458
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DOI: https://doi.org/10.1007/BF02279458