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Crystal structure of N-(4-nitrophenyl)-N-phenylsulfonamide

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Abstract

The crystal structure of N-(4-nitrophenyl)-N-phenylsulfonamide (C18H14N2O4S), a derivative of sulfonamide, has been determined by X-ray diffraction method using CuKα radiation. The compound crystallizes in the monoclinic space groupP21/n, witha=24.463(1),b=5.745(2),c=11.428(3)Å andβ=94.39(2)°. The structure was solved by direct methods and refined by full-matrix least squares to a finalR value of 0.045 with 3032 unique reflections. The dihedral angle between the substituents phenyl ring B and the phenyl A is 94.7(3)°. The S atom is in the usual distorted tetrahedral configuration.

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References

  • Abrahams, S. C. (1950)Acta Cryst. 3, 194.

    Google Scholar 

  • Basak, A. K., Mazumdar, S. K., and Choudhuri, S. (1982)Cryst. Struct. Common. 11, 1609.

    Google Scholar 

  • Basak, A. K., Mazumdar, S. K., and Choudruri, S. (1983)Acta Cryst. C 39, 492.

    Google Scholar 

  • Basak, A. K., Mazumdar, S. K., and Choudruri, S. (1984)Acta Cryst. C 40, 419.

    Google Scholar 

  • Basak, A. K., Choudhuri, S., and Mazumdar, S. K., (1984)Acta Cryst. C 40, 1848.

    Google Scholar 

  • Basak, A. K., Mazumdar, S. K., and Choudhuri, S. (1987)Acta Cryst. C 43, 735.

    Google Scholar 

  • Brown, G. M. (1971)Adv. Biochem. 35, 35.

    Google Scholar 

  • Camerman, A. (1970)Canad. J. Chem. 48, 179.

    Google Scholar 

  • Christoph, G. G., and Fleischer, E. B. (1973)Acta Cryst. B 29, 121.

    Google Scholar 

  • Cotton, F. A., and Stokley, P. F. (1970)J. Am. Chem. Soc. 92, 294.

    Google Scholar 

  • Ghosh, M., Basak, A. K., Mazumdar, S. K., and Sheldrick, B. (1989)J. Cryst. Spectro. Res. 19(2), 289.

    Google Scholar 

  • Kalman, A., Czugler, M., and Argay, Gy. (1981)Acta Cryst. B 37, 868.

    Google Scholar 

  • Nardelli, M. (1983)Comput. Chem. 7, 95.

    Google Scholar 

  • Shefter, E., Chmielewicz, Z. F., Blount, J. F., Brennan, T. F., Sackman, B. E., and Sackman, P. (1972)J. Pharmac. Sci. 61, 873.

    Google Scholar 

  • Sheldrick, G. M. (1986)SHELXS86. Program for the solution of crystal structure. (Univ. of Gottingen, Germany).

    Google Scholar 

  • Sheldrick, G. M. (1976)SHELX-76. Programs for crystal structure determination. Cambridge, England.

  • Trotter, J. (1959)Acta Cryst. 12, 884.

    Google Scholar 

  • Trotter, J. (1960)Tetrahedron 8, 13.

    Google Scholar 

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Author notes

  1. G. Biswas

    Present address: Department of Physics, Balurghat College, P.O.-Balurghat, Dist-South Dinajpur, West Bengal, India

Authors and Affiliations

  1. Biophysics Department, Bose Institute, Calcutta-54, India

    A. C. Gomes, G. Biswas, S. Biswas & Asok Banerjee

  2. Chemistry Department, Bose Institute, Calcutta-9, India

    G. K. Biswas

  3. Faculty of Pharmaceutical Sciences, Tokyo University, Bunkyo, 117, Tokyo, Japan

    Y. Iitaka

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  1. A. C. Gomes
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  2. G. Biswas
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  3. S. Biswas
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  4. G. K. Biswas
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  5. Y. Iitaka
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  6. Asok Banerjee
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Gomes, A.C., Biswas, G., Biswas, S. et al. Crystal structure of N-(4-nitrophenyl)-N-phenylsulfonamide. Journal of Crystallographic and Spectroscopic Research 23, 513–517 (1993). https://doi.org/10.1007/BF01182529

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  • DOI: https://doi.org/10.1007/BF01182529

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