ISSN:
0935-6304
Keywords:
Gas chromatography
;
Capillary, glass
;
Static coating
;
Filling with mechanical closure
;
Description of an easy and safe technique
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
The static technique is commonly accepted as the most universal and scientific method of coating. At the same time, however, it is said to be experimentally demanding. Great efforts have therefore been made to render the method easier and safer, resulting in a wealth of recommendations confusing non-experts. Over a period of two years we have practically applied most of the reported procedures with the aim of studying their practical convenience. We do not doubt that most procedures are comparably suitable in the hands of expert users, i. e. once the initiation efforts have been forgotten, or are otherwise of little interest. We have attempted to describe a method which is specifically suited for easy and quick introduction to beginners. The method is based on mechanical column closure. The principles of the method are discussed, and a comprehensive description of its practical application is given.
Additional Material:
5 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/jhrc.1240050302
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