ISSN:
1572-8854
Source:
Springer Online Journal Archives 1860-2000
Topics:
Geosciences
,
Physics
Notes:
Abstract The title compound, C16H24O4S3, crystallizes in the monoclinic system:a= 7.933(9) Å,b= 10.965(12) Å,c= 11.294(13) Å, β = 105.54(6) °,Z = 2, space groupP21 orP21/m. The structure could not be solved by direct methods in the former space group and was found to be disordered inP21/m with the molecule and its image mirrored aty= 1/4,3/4 occupying the same lattice site with occupancy 0.5.The manner in which molecular conflicts can be avoided in theP21/m structure is discussed. The molecular structure proposed by Praefcke et al. (1973) was confirmed.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF01270619
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