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  • 1
    ISSN: 1420-9136
    Schlagwort(e): High pressure ; pressure calibration ; ZnTe ; synchrotron X-ray source ; DIA type cubic anvil apparatus
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Geologie und Paläontologie , Physik
    Notizen: Abstract Pressure behavior of ZnTe at room temperature was studied using an X-ray energy dispersive method on a DIA type cubic anvil apparatus (SAM-85) at NSLS-X17B1. By using powdered polyethylene, the sample and NaCl for a pressure scale were held under quasihydrostatic conditions, which were confirmed by X-ray diffraction method. Two high-pressure phase transitions were confirmed using X-ray powder diffraction simultaneously with electrical resistance measurements. The phase transition pressures under quasihydrostatic conditions were determined to be 9.6 GPa, at which the resistance increased, and 12.0 GPa, which was the midpoint of a large resistance decrease. Errors in the pressure determinations were estimated to be less than 0.2 GPa. These pressure values may depend on grain size and anisotropic stress effects on the calibrant. From X-ray observation of ZnTe, the bulk modulus of the zinc blende structure was calculated to beK 0=51(3) GPa andK 0 ′ =3.6(0.8), and the first transition at 9.6 GPa was found to have about 9% volume change. It was consistent with an anomaly in the pressure generating curves.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 2
    Digitale Medien
    Digitale Medien
    Springer
    Pure and applied geophysics 146 (1996), S. 533-549 
    ISSN: 1420-9136
    Schlagwort(e): Lower mantle ; seismic tomography ; thermoelasticiti ; composition models ; geodynamics ; shear modulus
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Geologie und Paläontologie , Physik
    Notizen: Abstract We estimate (ϖμ/ϖT) P of the lower mantle at seismic frequencies using two distinct approaches by combining ambient laboratory measurements on lower mantle minerals with seismic data. In the first approach, an upper bound is estimated for |(ϖμ/ϖT) P | by comparing the shear modulus (μ) profile of PREM with laboratory room-temperature data of μ extrapolated to high pressures. The second approach employs a seismic tomography constraint (ϖ lnV S /ϖ lnV P ) P =1.8–2, which directly relates (ϖμ/ϖT) P with (ϖK S /ϖT) P . An average (ϖK S /ϖT) P can be obtained by comparing the well-established room-temperature compression data for lower mantle minerals with theK S profile of PREM along several possible adiabats. Both (ϖK S /ϖT) and (ϖμ/ϖT) depend on silicon content [or (Mg+Fe)/Sil of the model. For various compositions, the two approaches predict rather distinct (ϖμ/ϖT) P vs. (ϖK S /ϖT) P curves, which intersect at a composition similar to pyrolite with (ϖμ/ϖT) P =−0.02 to −0.035 and (ϖK S /ϖT) P =−0.015 to −0.020 GPa/K. The pure perovskite model, on the other hand, yields grossly inconsistent results using the two approaches. We conclude that both vertical and lateral variations in seismic velocities are consistent with variation due to pressure, temperature, and phase transformations of a uniform composition. Additional physical properties of a pyrolite lower mantle are further predicted. Lateral temperature variations are predicted to be about 100–250 K, and the ratio of (ϖ lnp/ϖ lnV S ) P around 0.13 and 0.26. All of these parameters increase slightly with depth if the ratio of (ϖ lnV S /ϖ lnV P ) P remains constant throughout the lower mantle. These predicted values are in excellent agreement with geodynamic analyses, in which the ratios (ϖ ln ϱ/ϖ lnV S ) P and (ϖ ϱ/ϖ lnV S ) P are free parameters arbitrarily adjusted to fit the tomography and geoid data.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 3
    Digitale Medien
    Digitale Medien
    College Park, Md. : American Institute of Physics (AIP)
    The Journal of Chemical Physics 114 (2001), S. 3809-3816 
    ISSN: 1089-7690
    Quelle: AIP Digital Archive
    Thema: Physik , Chemie und Pharmazie
    Notizen: The behavior of tethered polymers on gel/gel adhesion is studied with the single-chain mean-field (SCMF) theory. It is shown that the gel surface structure, the gel/gel adhesion strength, the equilibrium gel/gel distance, and the detailed interface structures can be tailored by specifically designed tethered layers on gel surfaces. The SCMF theory allows to study the effect of various variables of tethered layers, such as the surface coverage, the attraction between polymers and gels, and the composition of block copolymers. These theoretical results provide guidelines for experimental designs of novel gel materials with tethered layers. © 2001 American Institute of Physics.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 4
    Digitale Medien
    Digitale Medien
    Bradford : Emerald
    Industrial robot 32 (2005), S. 24-31 
    ISSN: 0143-991X
    Quelle: Emerald Fulltext Archive Database 1994-2005
    Thema: Maschinenbau
    Notizen: Purpose - Selection of an effective grasp of a complex object using a multifingered gripper is a challenging problem because of the many possible grasp positions that are typically available. Design/methodology/approach - Given the geometrical description of the particular object feature to be grasped, all feasible grasps are performed in offline simulation using a geometrically accurate model of the desired gripper. The six-dimensional convex hull for each grasp is computed and archived. This convex hull indicates the span of forces and torques that the grasp can resist. When a grasp is needed the force/torque due to the total object weight is estimated and the best grasp is selected. The selected grasp has minimum peak contact force consistent with equilibrium. Findings - Experimental trials with several complex object show the method is capable of producing grasps which can support the object and resist external force/torque. Research limitations/implications - An accurate geometrical description of the feature to be grasped must be known in advance. This would typically be a cylindrical or prismatic portion of the object. Practical implications - There are many environments in which a dexterous multifingered gripper must be used due to the variety of objects which must be grasped. The results indicate that effective grasps can be selected for complex objects from a database of simulated grasps. Originality/value - The primary contribution of this paper is the use of a database of simulated grasps on simple graspable features to synthesize grasps on complex objects.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 5
    Digitale Medien
    Digitale Medien
    Oxford, UK : Blackwell Publishing Ltd
    Journal of food science 62 (1997), S. 0 
    ISSN: 1750-3841
    Quelle: Blackwell Publishing Journal Backfiles 1879-2005
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft , Werkstoffwissenschaften, Fertigungsverfahren, Fertigung
    Notizen: A test chamber was designed and constructed and prechill chicken carcasses inoculated with Salmonella typhimurium were treated in it. They were sprayed with tap water, 0.85% sodium chloride (NaCl), 5% or 10% trisodium phosphate (TSP), 5% or 10% sodium bisulfate (SBS), 0.1% cetylpyridinium chloride (CPC), or 1% lactic acids (LAC) at 207, 345 or 827 kPa pressure for either 30 or 90 sec exposure time. Samples were taken from carcass wash water to determine the most probable number of Salmonella. Compared to tap water spraying, 0.85% NaCl spraying did not significantly reduce Salmonella. The greatest reductions of S. typhimurium, by 10% TSP, 10% SBS, 0.1% CPC or 1% LAC spraying, were 3.7, 2.4, 1.6 or 1.6 log in 90 sec treatments, respectively.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 6
    Digitale Medien
    Digitale Medien
    Oxford, UK : Blackwell Publishing Ltd
    Journal of food science 63 (1998), S. 0 
    ISSN: 1750-3841
    Quelle: Blackwell Publishing Journal Backfiles 1879-2005
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft , Werkstoffwissenschaften, Fertigungsverfahren, Fertigung
    Notizen: Chemical spray parameters, including temperature, pressure and exposure time, were evaluated for their effects on reducing Salmonella typhimurium on chicken skins. Pre-chilled chicken carcass skins were inoculated with S. typhimurium and sprayed with 0.1% cetylpyridinium chloride (CPC), 10% trisodium phosphate (TSP), or 2% lactic acid (LA). In the CPC spray, the 40°C treatments resulted in the greatest bacterial reduction. The most effective spray temperatures for LA and TSP treatments were 40 to 55°C. All chemical spray treatments at 207–1034 kPa reduced S. typhimurium. The reduction of S. typhimurium was greatest in all treatments when sprayed with 90 sec spray and 90 sec setting time.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 7
    ISSN: 1750-3841
    Quelle: Blackwell Publishing Journal Backfiles 1879-2005
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft , Werkstoffwissenschaften, Fertigungsverfahren, Fertigung
    Notizen: Chicken skins inoculated with Salmonella typhimurium at 1 × 108 CFU/mL were subjected to chemical or electrical treatments (4 mA/ cm2 current, 1 kHz frequency and 50% duty cycle) for 10 min in 1% sodium chloride (NaCl), sodium carbonate (Na2CO3), or trisodium phosphate (Na3PO4 12H2O or TSP). Salmonellae on chicken skins and in treatment solutions and rinsing water were enumerated with microbiological platings. Chicken skin was also examined using scanning electron microscopy.S. typhimurium attached to skins were reduced by 90% after electrical treatments in 1% NaCl, Na2CO3, or TSP, while the reduction ranged from 34% to 76% in groups treated by the salts alone.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 8
    ISSN: 1440-1738
    Quelle: Blackwell Publishing Journal Backfiles 1879-2005
    Thema: Geologie und Paläontologie
    Notizen: Abstract  The Yanbian area is located in the eastern part of the Central Asian Orogenic Belt (CAOB) of China and is characterized by widespread Phanerozoic granitic intrusions. It was previously thought that the Yanbian granitoids were mainly emplaced in the Early Paleozoic (so-called ‘Caledonian’ granitoids), extending east–west along the northern margin of the North China craton. However, few of them have been precisely dated; therefore, five typical ‘Caledonian’ granitic intrusions (the Huangniling, Dakai, Mengshan, Gaoling and Bailiping batholiths) were selected for U–Pb zircon isotopic study. New-age data show that emplacement of these granitoids extended from the Late Paleozoic to Late Mesozoic (285–116 Ma). This indicates that no ‘Caledonian’ granitic belt exists along the northern margin of the North China craton. The granitoids can be subdivided into four episodes based on our new data: Early Permian (285 ± 9 Ma), Early Triassic (249–245 Ma), Jurassic (192–168 Ma) and Cretaceous (119–116 Ma). The 285 ± 9 Ma tonalite was most likely related to subduction of the Paleo-Asian Oceanic Plate beneath the North China craton, followed by Triassic (249–245 Ma) syn-collisional monzogranites, representing the collision of the CAOB orogenic collage with the North China craton and final closure of the Paleo-Asian Ocean. The Jurassic granitoids resulted from subduction of the Paleo-Pacific plate and subsequent collision of the Jiamusi–Khanka Massif with the existing continent, assembled in the Triassic. The Early Cretaceous granitoids formed in an extensional setting along the eastern Asian continental margin.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 9
    Digitale Medien
    Digitale Medien
    Oxford, UK : Blackwell Science Ltd
    Geophysical prospecting 51 (2003), S. 0 
    ISSN: 1365-2478
    Quelle: Blackwell Publishing Journal Backfiles 1879-2005
    Thema: Geologie und Paläontologie , Physik
    Notizen: Wide-angle multicomponent ocean-bottom cable (OBC) data should further enhance sub-basalt imaging by using both compressional and converted shear wavefields. The first step in analysing multicomponent OBC data is to decompose the recorded wavefields into pure P- and pure S-wavefields, and extract the upgoing P- and S-waves. This paper presents a new scheme to separate P- and S-wavefields from wide-angle multicomponent OBC data in the τ–p domain. By considering plane-wave components with a known horizontal slowness, the P- and S-wavefields are separated into the directions of observed P- and S-wave oscillations using the horizontal and vertical components of the data. The upgoing P- and S-waves are then extracted from the separated P- and S-wavefields. The parameters used in the separation are the seismic wave velocities and the density at the receiver location, which can be estimated from the first reflection phase observed on the horizontal and vertical components. Numerical tests on synthetic data for a plane-layered model show good performance and demonstrate the accuracy of the scheme. Separation of wavefields from a basalt model is performed using synthetic wide-angle multicomponent OBC data. The results show that both near-offset and wide-angle reflections and conversions from within and below basalt layers are enhanced and clearly identified on the separated wavefields.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 10
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: We describe a laser heated diamond anvil cell system at the GeoSoilEnviroCARS sector at the Advanced Photon Source. The system can be used for in situ x-ray measurements at simultaneously ultrahigh pressures (to 〉150 GPa) and ultrahigh temperatures (to 〉4000 K). Design goals of the laser heating system include generation of a large heating volume compared to the x-ray beam size, minimization of the sample temperature gradients both radially and axially in the diamond anvil cell, and maximization of heating stability. The system is based on double-sided laser heating technique and consists of two Nd:YLF lasers with one operating in TEM00 mode and the other in TEM01* mode, optics to heat the sample from both sides, and two spectroradiometric systems for temperature measurements on both sides. When combined with an x-ray microbeam (3–10 μm) technique, a temperature variation of less than 50 K can be achieved within an x-ray sampled region for longer than 10 min. The system has been used to obtain in situ structural data and high temperature equations of state on metals, oxides, and silicates to 3500 K and 160 GPa. © 2001 American Institute of Physics.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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