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  • Filling with mechanical closure  (1)
  • Immobilization of moderately polar phases  (1)
  • Immobilized coatings  (1)
  • Wiley-Blackwell  (3)
  • 1980-1984  (3)
  • 1
    Digitale Medien
    Digitale Medien
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 5 (1982), S. 119-123 
    ISSN: 0935-6304
    Schlagwort(e): Gas chromatography ; Capillary, glass ; Static coating ; Filling with mechanical closure ; Description of an easy and safe technique ; Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The static technique is commonly accepted as the most universal and scientific method of coating. At the same time, however, it is said to be experimentally demanding. Great efforts have therefore been made to render the method easier and safer, resulting in a wealth of recommendations confusing non-experts. Over a period of two years we have practically applied most of the reported procedures with the aim of studying their practical convenience. We do not doubt that most procedures are comparably suitable in the hands of expert users, i. e. once the initiation efforts have been forgotten, or are otherwise of little interest. We have attempted to describe a method which is specifically suited for easy and quick introduction to beginners. The method is based on mechanical column closure. The principles of the method are discussed, and a comprehensive description of its practical application is given.
    Zusätzliches Material: 5 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 2
    Digitale Medien
    Digitale Medien
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 6 (1983), S. 153-155 
    ISSN: 0935-6304
    Schlagwort(e): Gas chromatography ; Capillary, glass ; Immobilization of moderately polar phases ; Combination of surface bonding and crosslinking ; Vinyl groups in the support surface ; Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Zusätzliches Material: 2 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
    BibTip Andere fanden auch interessant ...
  • 3
    Digitale Medien
    Digitale Medien
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 5 (1982), S. 349-354 
    ISSN: 0935-6304
    Schlagwort(e): Gas chromatography, capillary ; Persilylated, apolar columns ; Immobilized coatings ; Determination of column bleeding ; Re-silylation of fresh and used columns ; Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The bleeding of apolar high temperature columns may well be the critical factor limiting their applicability for GC/MS-coupling, and for high temperature analyses. Therefore, a bleeding determination procedure has been designed as a basis for a systematic approach to the production of low-bleed columns. Re-silylation is a traditional method of reducing column bleeding. Increased efficiency of re-silylation becomes feasible with immoblized coatings. Experience gained so far shows that resilylation of immoblized coatings may indeed result in the expected strongly reduced bleed rates and in improved overall column quality. Re-silylation may also contribute to column washing by enhancing the solubility of adsorbed contaminants.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
    BibTip Andere fanden auch interessant ...
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