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  • 1
    Electronic Resource
    Electronic Resource
    Springer
    International journal of thermophysics 19 (1998), S. 291-304 
    ISSN: 1572-9567
    Keywords: calorimetry ; emissivity ; high temperature ; specific heat capacity ; thermal conductivity
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract Thermal radiation calorimetry has been applied to measure the thermal conductivity and the specific heat capacity of an isolated solid specimen simultaneously. The system, in which a disk-shaped specimen and a flat heater are mounted in a vacuum chamber with the specimen heated on one face by irradiation, is presented. A theoretical formulation of the simultaneous measurement at quasi-steady state is described in detail. Noncontact temperature measurement of both specimen surfaces has been performed using pyrometers and a thermocouple set in the gap between the heater and the specimen. Pyroceram 9609 specimens, whose surfaces were blackened with colloidal graphite, were used in the measurement. The largest error involved in the noncontact temperature measurement is ±2°C in the range from 450 to 650°C. The resultant values of the specific heat capacity and the thermal conductivity deviate by about 10% from the recommended values for the Pyroceram specimen.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    International journal of thermophysics 20 (1999), S. 721-731 
    ISSN: 1572-9567
    Keywords: effective emissivity ; specific heat capacity ; thermal radiation calorimetry
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract A novel method for measurement of the specific heat capacity in the temperature range from 150 to 310 K is described. In order to achieve good temperature homogeneity in a disk-shaped specimen, a cylindrical heater was used in an apparatus based on thermal radiation calorimetry. A mixture of Bi2O3 and MgO powders was used for blackening the surfaces of the specimen, the heater, and the inside wall of the chamber. The specific heat capacities of Ni, fused quartz glass, and BaTiO3 ceramic were measured to test the performance of the calorimeter. Agreement to within 5% of the values published in the literature was obtained for these samples. Thermal hysteresis and anomalies associated with the first-order phase transition in BaTiO3 were detected in the present experiment.
    Type of Medium: Electronic Resource
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