ISSN:
1435-1536
Keywords:
Key words Emulsion polymerization
;
solid-state NMR spectroscopy
;
on-line detection
;
poly(butyl acrylate)
Source:
Springer Online Journal Archives 1860-2000
Topics:
Chemistry and Pharmacology
,
Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
Notes:
Abstract The on-line detection of emulsion polymerization processes by means of solid-state NMR spectroscopy is demonstrated for the first time using poly(butyl acrylate) as a model system. Relatively short time intervals are accessible via 1H detection while the use of 13C NMR spectroscopy results in an increased spectral resolution. Details of sample preparation and experimental techniques are given, while remaining artifacts of the preliminary results will be addressed in further investigations.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/s003960050251
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