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  • Chemistry  (31)
  • Organic Chemistry  (14)
  • Ion implantation  (2)
  • (Sea cucumber)  (1)
  • 1
    ISSN: 0304-4165
    Keywords: (Sea cucumber) ; Carbohydrate structure ; Fucose derivative ; Glycoprotein ; Neuraminic acid
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Biology , Chemistry and Pharmacology , Medicine , Physics
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    Applied physics 3 (1974), S. 321-324 
    ISSN: 1432-0630
    Keywords: Ion implantation ; Profiles ; Damage
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The important role of damage dependent electrical activation in the case of boron implanted silicon layers is whown by comparing measured acceptor concentration profiles in differently amorphized silicon layers. It is shown that the amorphous layer is completely recrystallized after a 650° C anneal for 10 min and the implanted boron is electrically active. In the heavily damaged but not amorphous region underneath the amorphous layer the implanted boron is hardly electrically active after this temperature treatment. At higher annealing temperatures the electrical activity increases, but 900° C are required for complete activation of the implanted boron. These results indicate that the process to activate the implanted boron electrically is strongly damage dependent. We thus found a new contribution to the understanding of the annealing behavior of implanted layers.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Springer
    Applied physics 4 (1974), S. 115-123 
    ISSN: 1432-0630
    Keywords: Ion implantation ; Backscattering ; Profiles
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Measurements of doping concentration and mobility of arsenic implanted silicon at high energies and at low energies with following drive-in diffusion are presented. The electrical measurements are compared with and supported by backscattering measurements. Tails which are present after short time anneals vanish during drive-in diffusion. A temperature of at least 825°C is required to fully activate the arsenic and to obtain the same mobility as in diffused samples. Backscattering data reveal an anomaly in the annealing behavior of the damage. After prolonged annealing As shows some accumulation at the surface. For drive-in diffusions lattice location experiments were performed.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    New York, NY [u.a.] : Wiley-Blackwell
    X-Ray Spectrometry 4 (1975), S. 85-89 
    ISSN: 0049-8246
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: The zinc concentration in an epitaxial layer of InSb was measured by proton excited X-rays. For the determination of zinc concentration, the X-ray yield was compared to that from known zinc concentrations. As layer thickness, stopping power and X-ray absorption must be taken into account, a general mathematical evaluation was developed. In an appendix, the derived equations are shown to allow a layer thickness determination. The calculated values agree quite well with the experimental results.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 441 (1978), S. 125-164 
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Formation of Organosilicon Compounds. 72. The Reactivity of Carbosilanes and their C-Chlorinated Derivatives in Reactions with CH3MgCl and LiCH3Reactions of (H3Si—CH2)2SiH2 1, (H2Si—CH2)3 2, (H3Si)2CCl2 3, (H3Si)2CHCl 4, H3Si—CCl2—SiH2-CH2-SiH3 5, and (H3Si—CCl2)2SiH2 6 as well as H3SiCH2Cl, H3SiCHCl2, and H3SiCCl3 with meMgCl and Lime (me = CH3) respectively are reported. In 1 and 2 by using tetrahydrofurane (THF) as a solvent, methylation to a higher degree is possible. The C-chlorination increases the activation of the Si—H group. Reactions of the C-chlorinated compounds result in Si—H substitution (maintaining of molecular frame), in cleavage and enlargement of the molecular frame and in transformation of CCl2 group into CHCl and CH2 groups respectively. Reactions with meMgCl in THF and with Lime in diethylether (Et2O) favour the cleavage of the molecular and the hydrogenation of the CCl2 group. The methylation of compound 5 occures on the Si—H groups neighbouring the CCl2 groups. The reactivity of these Si—H groups is decreased by increasing methylation. Reacting compound 6 with meMgCl in Et2O cleavage reations dominate. However, using cyclohexane as a solvent this cleavage reaction recedes in favour of the formation of 1,3,5-trisilapentane, containing a CCl2 group and a CHCl or a CH2 group. Thereby however, the methylation of only two SiH groups is observed. The 1H-, 29Si-, and 13C-n.m.r. data allow an assessment of progressing SiH-methylation within the homologous series.
    Notes: Es wird über Umsetzungen von (H3Si—CH2)2SiH2 1, (H2Si—CH2)3 2, (H3Si)2CCl2 3, (H3Si)2CHCl 4, H3Si—CCl2—SiH2—CH2-SiH3 5 und (H3Si—CCl2)2SiH2SiH2 6 sowie von H3Si—CH2Cl, H3Si—CHCl2, H3Si—CCl3 mit meMgCl bzw. Lime (me = CH3) berichtet. In 1 und 2 werden durch Verwendung von Tetrahydrofuran (THF) als Lösungsmittel höhere Methylierungsstufen ermöglicht. Die C-Chlorierung bewirkt eine Aktivierung der Si—H-Gruppe. Die C-chlorierten Verbindungen reagieren unter Si—H Substitution (Erhalt des Molekülgerüstes), unter Spaltungen und Vergrößerungen des Molekügerüstes und unter Hydrierung der CCl2-Gruppe zu der CHCl- bzw. CH2-Gruppe. Bei Umsetzungen mit meMgCl in THF oder mit Lime in Diäthyläther (Et2O) werden Reaktionen begünstigt, die unter Molekülspaltung und CCl2-Hydrierung ablaufen. In 5 beginnt die Methylierung an den der CCl2-Gruppe benachbarten SiH-Gruppen, deren Reaktionsfähigkeit mit steigendem Methylierungsgrad sinkt. Bei 6 bestimmen die Si—C-Spaltungen den Reaktionsablauf (Umsetzung mit meMgCl in Et2O), der aber durch Verwendung von Cyclohexan als Lösungsmittel zurückgedrängt wird zugunsten der Bildung von 1,3,5-Trisilapentanen mit einer CCl2- und einer CHCl- oder CH2-Gruppe, wobei aber nur maximal die Methylierung von zwei SiH-Gruppen erreicht wird. Die 1H-, 29Si- und 13C-NMR-Daten erlauben eine Abschätzung des Verlaufs der SiH-Methylierung innerhalb der homologen Reihen.
    Additional Material: 5 Ill.
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  • 6
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Zeitschrift für die chemische Industrie 55 (1942), S. 145-145 
    ISSN: 0044-8249
    Keywords: Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 3 (1972), S. 263-264 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: A simple Method for the Detection of soluble Auxiliary Agents containing Dimethylsilicone. Rapid detection of soluble dimethyl silicone compounds, occurring as residues of auxiliary agents or finishes on the surface of hardware, which in special cases may cause hazardous effects, can be achieved by a simple test. Since silicone compounds decrease the surface tension of trichloro-ethylene (TRI), shaking of such solutions produces foam. The stability of the foam depends on the silicone concentration from 10 μg silicone per ml TRI (detection limit) up to about 100 mg/ml TRI (saturation).
    Notes: Zum schnellen Nachweis löslicher Dimethylsilikonverbindungen, die auf Oberflächen von Bauteilen z. B. als Reste von Verarbeitungshilfsmitteln oder als Bestandteile von Lacken in bestimmten Fällen Ursache unerwünschter Effekte sein können, hat sich ein sog. „TRI-Schütteltest“ bewährt. Silikonverbindungen setzen die Oberflächenspannung von Trichloräthylen (TRI) herab, so daß beim Schütteln Schaum entsteht. Die Beständigkeit des Schaumes ist ein Maß für den Silikongehalt der Lösung zwischen 10 μg Silikon/ml TRI (Nachweisgrenze) und etwa 100 mg/ml TRI (Sättigung).
    Additional Material: 1 Ill.
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  • 8
    Electronic Resource
    Electronic Resource
    New York, NY : Wiley-Blackwell
    Helvetica Chimica Acta 37 (1954), S. 1080-1093 
    ISSN: 0018-019X
    Keywords: Chemistry ; Organic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Anhand von Experimenten mit radioaktiv markierten Stoffen liess sich zeigen, dass die thermische para-Claisen-Umlagerung von 2,6-Diallylphenyl-allyläther zu 2,4,6-Triallylphenol uber 2,2-Diallyl-6-allyl-cyclohexadienon-(l) als Zwischenprodukt verläuft. Dabei werden zwei cyclische Zwischenzustände durchschritten, die jedesmal eine Inversion der wandernden Allylgruppe bewirken.
    Additional Material: 1 Ill.
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  • 9
    Electronic Resource
    Electronic Resource
    New York, NY : Wiley-Blackwell
    Helvetica Chimica Acta 38 (1955), S. 783-789 
    ISSN: 0018-019X
    Keywords: Chemistry ; Organic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Es wurde mit Hilfe von radioaktiv indizierten Verbindungen gezeigt, dass die ortho-Claisen-Umlagerung von 2,4-disubstituierten Phenylallyläthern - im Gegensatz zu in 2-Stellung monosubstituierten Phenylallyläthern - einheitlich verläuft.
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  • 10
    ISSN: 0018-019X
    Keywords: Chemistry ; Organic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Bei der thermischen Umlagerung von [2-Propenyl-4,6-dimethyl-phenyl]-allyl-[γ-14C]-äther entst and ein 2-[P-Methyl-penta-α, δ-dienyl]-4,6-dimethyl-phenol, in welchem 84% der Radioaktivität im α- und 16% im γ-C-Atom der Pentadienyl-Seitenkette lokalisiert waren. Das Resultat eines Kreuzversuches spricht dagegen, dass diese Radioaktivitätsverteilung auf Radikalreaktionen zurückzuführen ist. Die möglichen unimolekularen Mechanismen dieser Seitenkettenumlagerung von Aryl-allyläthern aerden diskutiert.
    Additional Material: 1 Ill.
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