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Synthesis and Investigations on Nitrido(phthalocyaninato)rhenium Complexes (1999)

Frick, Karsten ; Ziener, Ulrich ; Hanack, Michael

Weinheim : Wiley-Blackwell

Berichte der deutschen chemischen Gesellschaft 1999 (1999), S. 1309-1313

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Details

ISSN: 1434-1948

Keywords: Phthalocyanines ; Rhenium ; Nitrido(octa-n-alkylphthalocyaninato)rhenium compounds ; Nucleophilic additions ; Chemistry ; General Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The reactions of nitrido(tetra-tert-butylphthalocyaninato)rhenium (1) with boron tribromide leading to (tBu4Pc)ReNBBr3 (4) and with acetone to give the imido complex (tBu4Pc)Re[NC(CH3)2CH2C(O)CH3]OH (2b) and its μ-oxo dimer 3 are reported. Starting from the corresponding 4,5-di-n-alkylphthalonitriles and ammonium perrhenate four soluble nitrido(octa-n-alkylphthalocyaninato)rhenium complexes 5-8 were synthesized. Nitrido(octa-n-pentylphthalocyaninato)rhenium (6) was treated with boron tribromide to afford [(C5H11)8Pc]ReNBBr3 (9).

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

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