ISSN:
1573-1111
Keywords:
N-tosyl-azamacrocycles
;
cyclophane
;
clathrate formation
;
synthetic routes
;
MS-fragmentation pattern
Source:
Springer Online Journal Archives 1860-2000
Topics:
Chemistry and Pharmacology
Notes:
Abstract The title compound, C41H40N2O6S2, has been synthesised in good yield and was found to form a 1∶1 inclusion compound with CHCl3 and other organic solvents. The crystal and molecular structure of the CHCl3 solvate has been determined by single crystal X-ray analysis and refined to anR-value of 0.034 for 3229 reflections. The compound is monoclinic, space groupP21/c, witha=15.316(1),b=14.515(1),c=18.720(3) Å, β=101.98(1)o, andZ=4. One molecule of chloroform is included in the crystal lattice.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF00709070
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