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  • 1
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    The influence of cobalt on the tensile and stress-rupture properties of the nickel-base superalloy MAR-M247 (1982)
    In:  Other Sources
    Details
    Publication Date: 2011-08-18
    Keywords: METALLIC MATERIALS
    Type: Metallurgical Transactions A - Physical Metallurgy and Materials Science; 13A; Oct. 198
    Format: text
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    NASA TECHNICAL REPORTS
  • 2
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    Fatigue and creep-fatigue deformation of several nickel-base superalloys at 650 C (1982)
    In:  Other Sources
    Details
    Publication Date: 2011-08-18
    Description: Transmission electron microscopy has been used to study the bulk deformation characteristics of seven nickel-base superalloys tested in fatigue and creep-fatigue at 650 C. The alloys were Waspalloy, HIP Astroloy, H plus F Astroloy, H plus F Rene 95, IN 100, MERL 76, and NASA IIB-7. The amount of bulk deformation observed in all the alloys was low. In tests with inelastic strain amplitudes less than about 0.003, only some grains exhibited yielding and the majority of those had the 110 line near the tensile axis. Deformation occurred on octahedral systems for all of the alloys except MERL 76 which also showed abundant primary cube slip. Creep-fatigue cycling occasionally produced extended faults between partial dislocations, but otherwise deformation was much the same as for fatigue cycling.
    Keywords: METALLIC MATERIALS
    Type: Metallurgical Transactions A - Physical Metallurgy and Materials Science; 13A; Oct. 198
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    NASA TECHNICAL REPORTS
  • 3
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    Microstructure and mechanical properties of bulk yttria-partially-stabilized zirconia (1981)
    In:  CASI
    Details
    Publication Date: 2019-06-28
    Description: A commercially available bulk 4.5 mole percent yttria-Y2O3)-partially-stabilized zirconia (PSZ) was studied by light microscopy, X-ray analysis, microhardness measurement, and fracture toughness testing. The growth of the precipitates and the phase transformations were studied as a function of aging in air at 1500 C. Aging cuves were constructed for both the as-received and the solution-annealed-and-quenched materials; the curves showed hardness peaks at 1397 and 1517 kg/sq mm, respectively. A total of twelve different types of tetragonal precipitates were found. The rectangular plate-shaped tetragonal precipitates were found to have a (110) habit plane. Grinding of the Y2O3 PSZ into powder did not cause a significant amount of metastable tetragonal precipitates to transform into the monoclinic phase, thus indicating that transformation toughening is not a significant mechanism for the material. The fracture toughness of the aged and of the unaged solution-annealed-and-quenched PSZ was found to be between 2 and 3 MN/cu m/2.
    Keywords: METALLIC MATERIALS
    Type: NASA-CR-165402
    Format: application/pdf
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    NASA TECHNICAL REPORTS
  • 4
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    Microstructure and mechanical properties of bulk and plasma-sprayed y2O3-partially stabilized zirconia (1980)
    In:  CASI
    Details
    Publication Date: 2019-06-28
    Description: Bulk 8.0 weight percent yttria partially stabilied zirconia (PSZ) was studied by light microscopy, transmission electron microscopy, X-ray analysis, microhardness testing, and fracture toughness testing. The as received PSZ contained spheroidal and grain boundary precipitates up to 4 micrometers in size. Spheroids up to 1.26 micrometers were metastable tetragonal; large spheroids were monoclinic. Grinding the PSZ into powder did not cause a significant amount of tetragonal to transform to monoclinic. This indicates that transformation toughness is not a significant mechanism in PSZ. Aging the PSZ at 1500 C caused the fine tetragonal precipitates to grow from 0.06 to 0.12 micrometers, in 250 minutes. A peak hardness of 1400 kg/sq mm was attained after 50 minutes. Solution annealing and quenching the as received PSZ eliminated the large precipitates, but fine tetragonal precipitates reformed on quenching. Aging at 1500 C caused the fine 0.02 micrometers tetragonal precipitates to grow into plates about 0.10 by 0.50 micrometers. A peak hardness of 1517 kg/sq mm was obtained after 250 minutes. On further aging, monoclinic percipitates formed along grain boundaries. The fracture toughness of the aged and unaged solution annealed and quenched PSZ was found to be between 2 and 3 MN /square root of m cubed. This range of fracture toughness is consistent with PSZ's that do not undergo transformation toughening.
    Keywords: METALLIC MATERIALS
    Type: NASA-CR-165126
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  • 5
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    Anisotropy of nickel-base superalloy single crystals (1980)
    In:  CASI
    Details
    Publication Date: 2019-07-13
    Description: The influence of orientation on the tensile and stress rupture behavior of 52 Mar-M247 single crystals was studied. Tensile tests were performed at temperatures between 23 and 1093 C; stress rupture behavior was examined between 760 and 1038 C. The mechanical behavior of the single crystals was rationalized on the basis of the Schmid factor contours for the operative slip systems and the lattice rotations which the crystals underwent during deformation. The tensile properties correlated well with the appropriate Schmid factor contours. The stress rupture lives at lower testing temperatures were greatly influenced by the lattice rotations required to produce cross slip. A unified analysis was attained for the stress rupture life data generated for the Mar-M247 single crystals at 760 and 774 C under a stress of 724 MPa and the data reported for Mar-M200 single crystals tested at 760 C under a stress of 689 MPa. Based on this analysis, the stereographic triangle was divided into several regions which were rank ordered according to stress rupture life for this temperature regime.
    Keywords: METALLIC MATERIALS
    Type: NASA-TM-81437 , E-327 , Intern. Symp. on Superalloys; Sep 21, 1980 - Sep 25, 1980; Champion, PA; United States
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  • 6
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    The influence of orientation on the stress rupture properties of nickel-base superalloy single crystals (1982)
    In:  Other Sources
    Details
    Publication Date: 2019-06-28
    Description: Constant load creep rupture tests were performed on MAR-M247 single crystals at 724 MPa and 774 C where the effect of anisotropy is prominent. The initial orientations of the specimens as well as the final orientations of selected crystals after stress rupture testing were determined by the Laue back-reflection X-ray technique. The stress rupture lives of the MAR-M247 single crystals were found to be largely determined by the lattice rotations required to produce intersecting slip, because second-stage creep does not begin until after the onset of intersecting slip. Crystals which required large rotations to become oriented for intersecting slip exhibited the shortest stress rupture lives, whereas crystals requiring little or no rotations exhibited the lowest minimum creep rates, and consequently, the longest stress rupture lives.
    Keywords: METALLIC MATERIALS
    Type: Metallurgical Transactions A - Physical Metallurgy and Materials Science; 13A; Oct. 198
    Format: text
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  • 7
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    The influence of cobalt on the microstructure of the nickel-base superalloy MAR-M247 (1982)
    In:  Other Sources
    Details
    Publication Date: 2019-06-28
    Description: Nickel was substituted for Co to produce 0, 5, and the standard 10% versions of MAR-M247, a cast nickel-base superalloy. The microstructures of the alloys were examined in as-cast, heat treated, aged, and stress-rupture tested conditions using a variety of metallographic techniques and differential thermal analysis. As cobalt concentration was reduced from 10 to 0 wt %, the gamma-prime weight fraction decreased from 59 to 41%; W and Ti concentrations in the gamma-prime phase increased from 5 to 8 and 2 to 3 at.%, respectively; the mean gamma-prime particle size increased from 0.6 to 0.8 micron; Cr and Al concentrations in the gamma matrix decreased from 17 to 13 and 15 to 12 at.%, respectively; and the weight fraction of carbides increased by approximately 1%.
    Keywords: METALLIC MATERIALS
    Type: Metallurgical Transactions A - Physical Metallurgy and Materials Science; 13A; Oct. 198
    Format: text
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  • 8
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    Anisotropy of nickel-base superalloy single crystals (1980)
    In:  Other Sources
    Details
    Publication Date: 2019-07-27
    Description: The effects of crystal orientation on the mechanical properties of single crystals of the nickel-based superalloy Mar-M247 are investigated. Tensile tests at temperatures from 23 to 1093 C and stress rupture tests at temperatures from 760 to 1038 C were performed for 52 single crystals at various orientations. During tensile testing between 23 and 760 C, single crystals with high Schmid factors were found to be favorably oriented for slip and to exhibit lower strength and higher ductility than those with low Schmid factors. Crystals which required large rotations to become oriented for cross slip were observed to have the shortest stress rupture lives at 760 C, while those which required little or no rotation had the longest lives. In addition, stereographic triangles obtained for Mar-M247 and Mar-M200 single crystals reveal that crystals with orientations near the -111 had the highest lives, those near the 001 had high lives, and those near the 011 had low lives.
    Keywords: METALLIC MATERIALS
    Type: International Symposium on Superalloys; Sept. 21-25, 1980; Champion, PA
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