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Digitale Medien

Elektronenkristallographie - jetzt eine gut zugängliche Methode (1997)

Mertin, Wilhelm

Weinheim : Wiley-Blackwell

Zeitschrift für die chemische Industrie 109 (1997), S. 46-48

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ISSN: 0044-8249

Schlagwort(e): Elektronenbeugung ; Elektronenkristallographie ; Elektronenmikroskopie ; Bildbearbeitung ; Strukturbestimmung ; Chemistry ; General Chemistry

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Zusätzliches Material: 1 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/ange.19971090107

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Digitale Medien

Preparation by ion milling and TEM investigation of embedded needle-shaped crystals of H-Nb2O5 (1991)

Krumeich, Frank ; Mertin, Wilhelm

New York, NY : Wiley-Blackwell

Journal of Electron Microscopy Technique 19 (1991), S. 361-365

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ISSN: 0741-0581

Schlagwort(e): Dimple grinder ; PIMS ; Amorphous surface layer ; Life and Medical Sciences ; Cell & Developmental Biology

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Allgemeine Naturwissenschaft

Notizen: A method for preparing needle-shaped and platelike crystals for electron microscopical investigation was elaborated. Crystals of H-Nb2O5 were embedded in a synthetic resin and disks were cut off perpendicular to the desired direction of observation. The thickness of the sample was reduced by planar grinding and then by using a dimple grinder and furthermore by ion milling with argon ions. With the precision ion milling system small crystal areas were selected and subsequently irradiated. The TEM investigations showed that the desired crystallographic orientation was reached and that the crystal structure has been preserved. The contrast of highly resolved images was reduced by an amorphous surface layer which was not removable.

Zusätzliches Material: 3 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/jemt.1060190310

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