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Nuclear magnetic resonance and infrared spectral characterization of some peroxysterols (1988)

Jaworski, Krzysztof ; Smith, Leland L.

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 26 (1988), S. 104-107

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ISSN: 0749-1581

Keywords: Cholesterol ; Peroxysterol ; Hydroperoxide ; Epidioxide ; Hydrogen bond ; Low-field proton signals ; Infrared ; 13C NMR spectra ; Proton spectra ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Proton and infrared absorption spectra of seven peroxysterols of general structure 6ξ-alkoxy-5,6ξ-epidioxy-5ξ-5,6-secocholestane-3β,5-diol reveal low-field (δH 10.0-10.8) sharp one-proton singlets and associated sharp 3280-3330 cm-1 absorption bands of the 5ξ-hydroxy group, intramolecularly hydrogen bonded to vicinal peroxide oxygen in a previously unrecognized correlation. The peroxysterols are also characterized by 13C NMR spectra.

Additional Material: 3 Tab.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260260203

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