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  • 1
    Publication Date: 2023-02-14
    Description: Abstract
    Description: A low blank, high-precision, and highly reproducible technique for Boron (B) isotope analysis performed by Multi-Collector-Inductively Coupled Plasma-Mass Spectrometer (MC-ICP-MS), Thermo Scientific Neptune PlusTM was developed and is presented here. We show data on a set of international certified standard materials (NIST SRM 951) and various kind of matrices (B1-IAEA, B2-IAEA, B3-IAEA, B4-IAEA, B5-IAEA, and JB-2) measured with MC-ICP-MS Neptune Plus, focusing on the accuracy and reproducibility of the analyses performed in the Neptune-TIMS Laboratory
    Keywords: Boron Isotopes ; MC-ICP-MS ; Neptune ; EPOS ; multi-scale laboratories ; geochemistry and microscopy ; geochemistry data ; EARTH SCIENCE 〉 SOLID EARTH 〉 GEOCHEMISTRY 〉 GEOCHEMICAL PROPERTIES ; In Situ/Laboratory Instruments 〉 Spectrometers/Radiometers 〉 MC-ICP-MS
    Type: Dataset , Dataset
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  • 2
    Publication Date: 2023-02-14
    Description: Abstract
    Description: Results of a high throughput, robust and sensitive method for the precise analysis of 87Sr/86Sr by Multi-Collector-Inductively Coupled Plasma-Mass Spectrometer (MC-ICP-MS), Thermo Scientific Neptune PlusTM are reported. The data were obtained after accurate procedures of chemical separation and purification of Sr from geological matrices such as silicates, sulfides, carbonates and waters, using Eichrom Sr-spec resins as well as the routine for Sr isotope measurement. Mass discrimination and instrument drift were corrected by using natural constant 86Sr/88Sr ratios as an internal standard. Data on set of international certified standard materials (SRM NIST 987 and AGV-1) as well as intra-lab reference samples (water sample KGV-9) measured with MC-ICP-MS Neptune Plus, focusing on the accuracy and reproducibility of the analyses performed in the Neptune-TIMS Laboratory are here reported.
    Keywords: Strontium Isotope ; MC-ICP-MS ; Neptune ; Isotope Ratios ; EPOS ; multi-scale laboratories ; geochemistry and microscopy ; geochemistry data ; EARTH SCIENCE 〉 SOLID EARTH 〉 GEOCHEMISTRY 〉 GEOCHEMICAL PROPERTIES ; In Situ/Laboratory Instruments 〉 Spectrometers/Radiometers 〉 MC-ICP-MS
    Type: Dataset , Dataset
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  • 3
    Publication Date: 2023-02-14
    Description: Abstract
    Description: We describe here in detail the results and the setup of the high precision Nd isotope ratio analysis performed by Multi Collector Inductively Coupled Plasma Mass Spectrometer (MC ICP MS), Thermo Scientific Neptune Plus TM. Isobaric interferences and mass discrimination were corrected by using natural invariable 147Sm/144Sm and 146Nd/144Nd isotope ratios. We reported data on set of international certified standard materials (JNdi-1 and AGV-1) measured with MC-ICP-MS Neptune Plus, focusing on the accuracy and reproducibility of the analyses performed in the Neptune-TIMS Laboratory
    Keywords: Neodymium Isotope ; MC-ICP-MS ; Neptune ; EPOS ; multi-scale laboratories ; geochemistry and microscopy ; geochemistry data ; EARTH SCIENCE 〉 SOLID EARTH 〉 GEOCHEMISTRY 〉 GEOCHEMICAL PROPERTIES ; In Situ/Laboratory Instruments 〉 Spectrometers/Radiometers 〉 MC-ICP-MS
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  • 4
    Publication Date: 2023-02-14
    Description: Abstract
    Description: We describe here in detail the results and the setup of the high precision Pb isotope ratio analysis performed by Multi Collector Inductively Coupled Plasma Mass Spectrometer (MC ICP MS), Thermo Scientific Neptune Plus TM. We performed this method adding thallium (Tl) as an internal isotopic standard to correct mass dependent isotopic fractionation. We also report the procedures for the chemical separat ion and purification of Pb from geological matri ces such as silicates , sulfides and historical artefacts . We report the data obtained on the international certified standard material SRM NIST 981 measured with MC ICP MS Neptune Plus, focusing on the accuracy and reproducibility of the analyses performed in the Neptune TIMS Laboratory (IGG-CNR in Pisa, Italy), and highlighting the advantages brought by the installation of this new mass spectrometer.
    Keywords: Lead Isotopes ; MC-ICP-MS ; Neptune-TIMS Laboratory ; Isotope Ratios ; EPOS ; multi-scale laboratories ; geochemistry and microscopy ; geochemistry data ; EARTH SCIENCE 〉 SOLID EARTH 〉 GEOCHEMISTRY 〉 GEOCHEMICAL PROPERTIES ; In Situ/Laboratory Instruments 〉 Spectrometers/Radiometers 〉 MC-ICP-MS
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  • 5
    Publication Date: 2021-05-12
    Description: We describe the results from an electrical resistivity tomography (ERT) survey performed inside the Solfatara cra- ter, located in the central part of the Campi Flegrei (CF) com- posite caldera. The Solfatara volcano represents the most ac- tive zone within the CF area, in terms of hydrothermal mani- festations and local seismicity. Eight dipole-dipole ERT lines have been measured with the aim of deducing a 3D resistivity model for the upper 80 m beneath the Solfatara. The results have allowed classification of the shallow structure below the crater into a low-resistivity (LR) class, up to about 4 Ωm, an intermediate resistivity (IR) class, from 5 Ωm up to 50 Ωm, and a high-resistivity (HR) class, from 60 Ωm onward. In order to solve the ambiguities arising in the interpretation of the nature of these bodies, a comparison has been done be- tween the 3D ERT model and the CO2 flux, soil temperature, and gravity maps over the same area. By combining all of these parameters, the whole LR body has been ascribed to a water-dominated geothermal basin and the HR body to a steam/gas-dominated reservoir. Finally, the IR class has been interpreted as a widespread background situation with inter- mediate character, where volatiles and condensates can coex- ist in the same volumes at variable percentages, coherently with the resistivity variation within this class. Since fluid dy- namics in the Solfatara crater change rapidly, ERT surveys repeated in the future are expected to be of great help in mon- itoring possible pre-eruptive changes, as well as in better fol- lowing evolution of the local geothermal system.
    Description: Published
    Description: 27
    Description: 2V. Struttura e sistema di alimentazione dei vulcani
    Description: JCR Journal
    Keywords: Campi Flegrei ; 3D resistivity tomography ; Near-surface structure ; Solfatara crater ; 04.02. Exploration geophysics
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 6
    Publication Date: 2017-04-04
    Description: x
    Description: Published
    Description: Trieste
    Description: 3.6. Fisica del vulcanismo
    Description: open
    Keywords: Campi Flegrei Deep Drilling Project ; Campi Flegrei ; Magma-water interaction ; 03. Hydrosphere::03.04. Chemical and biological::03.04.06. Hydrothermal systems
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: Poster session
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  • 7
    Publication Date: 2018-03-19
    Description: We describe the results from a combined controlled source audio magnetotelluric (CSAMT) and natural source magnetotelluric (MT) survey carried out in the Solfatara–Pisciarelli (S–P) area, located in the central part of the Campi Flegrei (CF) composite caldera, west of Naples, Southern Italy. The S–P area represents the most active zone within the CF caldera, in terms of hydrothermal manifestations and local seismicity. Since 1969, the CF caldera is experiencing ground deformation, seismicity and geochemical fluid changes, which are particularly ev- ident in the S–P area. A 1 km long, nearly W–E directed CSAMT–MT profile crossing the fumarole field was carried out in the S–P area with the aim of deducting a resistivity model of the structural setting of the hydrothermal system in the first 3 km depth. An interpretation of the modelled section across the profile is given in this paper, taking advantage from already existing seismic, gravity and geochemical data in the same area. Three well distinct zones have been outlined. The first zone is a very shallow, electrically conductive body localized be- neath the westernmost segment of the profile, which, within a short distance of about 100 m, dips westwards from near surface down to some hundred metres in depth. Mostly accounting for the very low resistivity (1–10 Ω m) and the exceedingly high values of vP/vS (N4), this shallow zone has been ascribed to a water- saturated, high-pressurized geothermal reservoir. The second zone, which has been localized below the west- central portion of the CSAMT–MT transect, appears as a composite body made up of a nearly vertical plumelike structure that escapes at about 2.25 km depth from the top edge of the east side of a presumably horizontal plate- like body. The plumelike structure rises up to the free surface in correspondence of the fumarole field, whereas the platelike structure deepens at least down to the 3 km of maximum exploration depth. The combined interpretation of resistivity (50–100 Ω m), body wave velocity ratio (vP/vS b 2.0), mass density contrast (Δσ b 0 g/cm3), and geochemical data indicates that the plumelike portion can likely be associated with a steam/gas- saturated column and the platelike portion with a high temperature (N300 °C), over-pressurized, gas- saturated reservoir. Finally, the third zone, which has been localized beneath the eastern half of the transect, from about 1.2 km down to about 3 km of depth, is also characterized by very low resistivity values (1–10 Ω m). Jointly interpreted with seismic (vP/vS b 1.73) and gravity (⨂ N 0 g/cm3) data, this last electrically conduc- tive structure appears to be associated with a hydrothermally mineralized, clay-rich body.
    Description: Published
    Description: 9-21
    Description: 2V. Struttura e sistema di alimentazione dei vulcani
    Description: JCR Journal
    Keywords: Magnetotelluric Hydrothermal system ; Volcano ; Campi Flegrei ; Hydrothermal system ; 04.02. Exploration geophysics
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 8
    Publication Date: 2022-06-14
    Description: This study focuses on the Solfatara volcano within Campi Flegrei, a volcanic eld located on the Tyrrhenian coast of southern Italy. Volcanism at the Campi Flegrei caldera has included phreatic to phreatomagmatic explosions and both magmatic (ranging from small scoria-producing events to those with Plinian columns) and effusive eruptions. These eruptions have formed tuff cones, tuff rings, minor scoria cones, and lava domes. A detailed stratigraphic, structural, and geo- physical study of the area indicates that the Solfatara volcano is a maar-diatreme structure previously not recognized within the Campi Flegrei caldera. It is characterized by a crater cut into earlier volcanic deposits, a small rim of ejecta, and a deep structure (down to 2–3 km). This maar-diatreme has allowed the gases and uids to ow up to the surface over a long time. A new geological map and cross sections show a complex architecture of different volcano-tectonic features including scoria cones, lavas, crypto- domes, feeder dikes, pipes, ring and regional faults, and explosive craters. Volcanological data were collected with the main aim of characterizing the eruptive activity in a lim- ited sector of the caldera. Fault and fracture analyses, using the scan line methodology, highlight the role of the main structures that accompanied the volcanic evolution within this sector of the Campi Flegrei caldera. To better constrain the subsurface structure of the Solfatara crater, electrical resistivity tomography investigations were integrated with the volcano-tectonic information. All data suggest that the Solfatara area is dominated by a maar-diatreme evolution. Pres- ently, the Solfatara area shows widespread hydrothermal and fumarolic activity that is localized along the major faults. The results allow us to de ne a particular type of vol- canic activity in the recent past, in what is still considered today an area with a higher probability of opening new vents, particu- larly for possible phreatic activity.
    Description: Published
    Description: 1485–1504
    Description: 2V. Struttura e sistema di alimentazione dei vulcani
    Description: JCR Journal
    Keywords: Solfatara volcano ; maar-diatreme ; Campi Flegrei ; electrical resistivity tomography ; 04.08. Volcanology
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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