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  • ASTROPHYSICS  (3)
  • Gas liquid chromatography (GLC)  (1)
  • DDR
  • Condensed Matter: Electronic Properties, etc.
  • 1985-1989  (4)
  • 1
    Digitale Medien
    Digitale Medien
    Quantitative analysis of ethylenediamine in plasma by capillary column gas chromatography (1986)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 9 (1986), S. 548-554 
    Details
    ISSN: 0935-6304
    Schlagwort(e): Gas liquid chromatography (GLC) ; Fused silica capillary columns ; Alkali flame ionization detection (AFID) ; Mass spectrometry (MS) ; Quantitation in human serum ; Ethylenediamine ; Aminophylline ; Small molecular weight amines and diamines ; m-Toluoyl derivatives ; Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: A specific and sensitive method for the determination of ethylenediamine in human plasma is described. The aqueous sample is treated with m-toluoyl chloride, yielding the N,N′-bis(m-toluoyl) derivative of the diamine, which is extracted into dichloromethane and quantitated after “on column” methylation by capillary gas liquid chromatography with alkali flame ionization detection. The corresponding derivative of putrescine serves as internal standard. The assay is reproducible and calibration curves are linear over the concentration range 0.05 to 10 μg · ml-1. The lower detection limit is about 10 ng · ml-1. The structures of the compounds of interest eluting from the capillary column are examined by gas liquid chromatography/mass spectrometry. The assay has been applied to the analysis of ethylenediamine in plasma following the administration of aminophylline and ethylenediamine in a cross-over study to patients with bronchopulmonary diseases. The method also proves suitable for measuring other primary and secondary amines and diamines in aqueous solutions by gas liquid chromatography.
    Zusätzliches Material: 7 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/jhrc.1240091002
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  • 2
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    High-resolution CCD imaging and derived gravitational lens models of 2237+0305 (1988)
    In:  Other Sources
    Details
    Publikationsdatum: 2019-07-12
    Beschreibung: Images of the gravitational lens 2237+0305 acquired in good seeing have resolved the system into at least five components within the central few arsec of the object: the galaxy nucleus and four point sources in a ringlike formation approximately centered on the galaxy. It is found that the four point sources are distinctly bluer than the galaxy, but that they do not have identical colors. The observed configuration is well reproduced by a simple model that assumes that the four objects are images of the quasar and that the lens is a constant mass-to-light ratio, elliptical, de Vaucouleurs bulge.
    Schlagwort(e): ASTROPHYSICS
    Materialart: Astronomical Journal (ISSN 0004-6256); 95; 1619-162
    Format: text
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  • 3
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    Spectroscopy of the extranuclear line-emitting regions associated with the gravitational lens system 2016 + 112 (1987)
    In:  Other Sources
    Details
    Publikationsdatum: 2019-07-12
    Beschreibung: Moderate-resolution slit spectroscopy of the extended emission-line objects A1 and B1 located within 5 arcsec of the triple radio source 2016 + 112 shows that at least one is physically associated with the z = 3.273 quasar thought to be multiply imaged by a foreground galaxy. The data and theoretical models unanimously favor the identification of A1 and B1 with two separate clouds of ionized gas that lie within a few kiloparsecs of the primary A/B QSO and radio source. The available evidence does not support the view that they are multiple images of a single object or their classification as separate (companion) galaxies.
    Schlagwort(e): ASTROPHYSICS
    Materialart: Astronomical Journal (ISSN 0004-6256); 94; 12-15
    Format: text
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  • 4
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    Spectroscopic CCD surveys for quasars at large redshift. I - A deep PFUEI survey (1986)
    In:  Other Sources
    Details
    Publikationsdatum: 2019-07-12
    Beschreibung: A survey for faint quasars has been conducted using slitless spectroscopy with the PFUEI at the 200 inch (5 m) telescope. The survey covers a total of 0.91 sq deg in 113 fields at galactic latitudes above 30 deg. Calibrated spectra in the range 4500-7200 A were obtained for more than 9000 objects. Emission-line candidates were selected on the basis of two criteria: the equivalent width must exceed 50 A, and the signal-to-noise ratio of the detection of the line versus the sky background should be larger than 7. Among 45 candidates so selected, subsequent slit spectroscopy confirmed 27 emission-line objects. Among these, 17 are emission-line galaxies with redshifts in the range 0.04-0.31, and 10 are quasars with redshifts between 0.91 and 2.66. The well-defined selection criteria for these objects, together with the distribution of rest frame equivalent widths of the emission lines, allow derivation of the area of sky covered as a function of the continuum limiting magnitude. The observed number of quasars in the redshift range 0.7-2.7 agrees well with that predicted by the luminosity function models published by Schmidt and Green in 1983. It is concluded that quasars with an absolute magnitude of M(B) = -25 suffer a redshift cutoff near or below a redshift of 3.
    Schlagwort(e): ASTROPHYSICS
    Materialart: Astrophysical Journal, Part 1 (ISSN 0004-637X); 306; 411-427
    Format: text
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