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Optimization of a GC-MS/MS Method for the Analysis of PCDDs and PCDFs in Human and Fish Tissue (2000)

Grabic, Roman ; Novák, Jaromír ; Pacáková, Vera

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 23 (2000), S. 595-599

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ISSN: 0935-6304

Keywords: GC-MS/MS ; PCDDs ; PCDFs ; human tissue ; fish tissue ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: ---This paper outlines the possibilities of selectivity and sensitivity enhancement in measuring PCDD/F congeners using an ion trap GC-MS/MS. The pressure of the collision gas and the collision energy were optimized. The modified GC-MS/MS method was applied to the determination of PCDDs and PCDFs in human and fish tissues. Limits of quantification were about 1 pg/g of fat for all seventeen 2378 PCDD/Fs tested (starting amount of fat, 2 g).

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

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