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  • Electron irradiation damage  (2)
  • Amorphous  (1)
  • 1
    Digitale Medien
    Digitale Medien
    New York, NY : Wiley-Blackwell
    Journal of Electron Microscopy Technique 3 (1986), S. 45-56 
    ISSN: 0741-0581
    Schlagwort(e): High voltage electron microscopy ; High resolution electron microscopy ; Amorphous ; Amorphization ; Niti alloy ; Mosaic block ; Electron irradiation damage ; Life and Medical Sciences ; Cell & Developmental Biology
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Allgemeine Naturwissenschaft
    Notizen: Amorphization induced by electron irradiation in Ni-50 at% Ti crystals has been investigated by electron microscopy. In order to clarify successive stages of amorphization, micrographs were taken in vairous regions where the total dose of electrons was continuously changed. Contrast was manipulated by changing the reflecting condition. Results obtained are summarized as follows: (a) Amorphization occurs inhomogenously; (b) there is a critical size, i.e., about 5 nmø in the crystals, for observing sharp lattice images in small blocks; (c) lattice images change to short and wavy fringe contrasts when the block size becomes smaller than the critical one, and finally they disappear; and (d) boundary contrast of the blocks rapidly decreases with decreasing size, and is hardly observed when the size becomes smaller than the critical one. Based on the results, the cause of abnormal fringe contrasts in fine blocks, the amorphization process, and atomic structures of amorphous materials are discussed.
    Zusätzliches Material: 7 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 2
    Digitale Medien
    Digitale Medien
    New York, NY : Wiley-Blackwell
    Journal of Electron Microscopy Technique 12 (1989), S. 201-218 
    ISSN: 0741-0581
    Schlagwort(e): Very-high-temperature stage ; Electron irradiation damage ; In situ deformation ; Ductile ceramics ; Amorphization ; Foreign atom implantation ; Environment - material interaction ; Life and Medical Sciences ; Cell & Developmental Biology
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Allgemeine Naturwissenschaft
    Notizen: High-voltage electron microscopy has shown itself advantageous for the study of natural science, including biology, but especially for materials science. The most important advantage for materials science is for in situ experiments about the detailed processes of the phenomena that occur in bulk materials. The present paper is mainly concerned with several types of in situ experiments that have been carried out in the Research Center for Ultra-High Voltage Electron Microscopy, Osaka University. The following subjects have been studied: (a) fundamental problems, such as the conditions necessary for in situ experiments, functional features of specimen treatment devices, and the effects of electron irradiation; (b) the dislocation behavior of crystals under various conditions; (c) high-temperature behavior of refractory materials, mainly ceramic composites; (d) new applications of electron irradiation effects, such as amorphization of crystalline materials and electron-irradiation-induced foreign-atom implantation; (e) environment-matter interaction, mainly chemical amorphization of alloys; and (f) future trends of the in situ experiment, such as combinations with Auger valency electron spectroscopy and high-resolution electron microscopy.
    Zusätzliches Material: 18 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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