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Spin density distribution in dialkyl oxalate radical anionsESR Studies on Carboxylic Esters, Part 9. For Part 8, see Ref. 1. (1988)

Brix, P. ; Helling, D. ; Voss, J.

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 26 (1988), S. 324-326

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ISSN: 0749-1581

Keywords: Dialkyl oxaltes ; Radical anions ; Isotropic ESR ; Anisotropic ESR ; 2H-, 13C-, 17O-Labelling ; MO calculations ; Spin densities ; E/Z Isomers ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The isotropic and anisotropic ESR spectra of dialkyl oxalate radical anions, including derivatives which were labelled with 13C or 17O in the carbonyl and 2H or 13C in the alkyl groups, were measured. The spin density distribution as determined from the experimental nuclear hyperfine coupling constants agrees very well with MNDO-CI calculations. As a consequence of the strictly planar structure of the radical anions, E/Z isomers are observed.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260260410

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