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Synthesis of vinyl-substituted oxiranes and their transformation to dihydrofurans (1994)

Popkov, S. V. ; Kovalenko, L. V. ; Tashchi, V. P. ; [et al.]

Springer

Russian chemical bulletin 43 (1994), S. 1363-1367

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ISSN: 1573-9171

Keywords: 2-methylcyclohexanone ; aromatic and heterocyclic aldehydes ; Claisen—Schmidt reaction ; C-methylation ; Corey—Chaykovsky reaction ; spirooxiranes ; substituted hexahydroisobenzofurans

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Abstract The reaction of dimethylsulfonium methylide with the carbonyl function of 2-arylidene-cyclohexanones obtained from 2-methylcyclohexanone affords the corresponding spirooxiranes. The application of this reaction to 2,2-dimethyl-6-(5-methylfurfurylidene)cyclohexanone and 2,2-dimethyl-6-(5-chlorofurfurylidene)cyclohexanone leads to substituted 4,4-dimethyl-1-furyl-1,-3,4,5,6,7-hexahydroisobenzofurans.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00703695

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