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  • 1
    Electronic Resource
    Electronic Resource
    Nonacarbonylbis(μ3-methylidin)trieisen (1990)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 123 (1990), S. 1481-1484 
    Details
    ISSN: 0009-2940
    Keywords: Alkylidyne complexes ; Clusters ; Halogen exchange reaction ; Iron complexes ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Nonacarbonylbis(μ3-methylidyne)triironHalogen exchange reaction in Fe3(CO)9(μ3—CF)2 (1) with BBr3 (3) yields Fe3(CO)9(μ3—CBr)2 (4), which can be converted by (C4H9)3SnH (5) into Fe3(CO)9(μ3—CH)2 (6). 6 is the parent compound of the bis(alkylidyne)triiron clusters. Selective reduction of the CBr moiety in Fe3(CO)9(μ3—CBr) (μ3—CCO2CH3) (7) results in the formation of Fe3(CO)9(μ3—CH) (μ3—CCO2CH3) (8). The structure of 8 has been elucidated by an X-ray crystalstructure determination.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19901230707
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  • 2
    Electronic Resource
    Electronic Resource
    Decacarbonyl(μ3;-η2-‖-1,4-dimethoxy-2-butyne)triiron, an Iron Cluster with Unusual Structure (1991)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 124 (1991), S. 773-775 
    Details
    ISSN: 0009-2940
    Keywords: Alkyne complexes ; Clusters ; Iron complexes ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Reaction of undecacarbonyl(acetonitrile)triiron (1) with 1,4-dimethoxy-2-butyne (2) yields the alkyne complexes decacarbonyl(μ3;-η2-Verbar-1,4-dimethoxy-2-butyne)triiron (3) and nonacarbonyl(μ3;-η2;-⊥-1,4-dimethoxy-3-butyne)triiron (4). The crystal structure determination of 2 shows that the alkyne ligand is coordinated strictly parallel to one iron-iron edge.
    Additional Material: 1 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19911240417
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  • 3
    Electronic Resource
    Electronic Resource
    Undecacarbonyl(μ2-trifluoromethyl isocyanide)triruthenium, a Derivative of [Ru3(CO)12] with [Fe3(CO)12] Structure (1991)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 124 (1991), S. 777-779 
    Details
    ISSN: 0009-2940
    Keywords: Trifluoromethyl isocyanide ligands ; Clusters ; Ruthenium complexes ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: [Ru3(CO)10(μ2-CO)(μ2-CNCF3)] (1), [Ru3(CO)10(CNCF3)2] (2), and [Ru2(CO)6(μ2-CNCF3)3] (3) are obtained by the reaction of [Ru3(CO)11(CH3CN)] with CNCF3. An X-ray crystal structure determination revealed, that 1 has an unusual [Fe3(CO)12] structure, different from most other derivatives of [Ru3(CO)12].
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19911240418
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