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  • Chemistry  (1)
  • 1965-1969  (1)
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  • 1
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 351 (1967), S. 63-67 
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Deutero iron(III) oxide hydroxide of goethite type, α-FeOOD, has been prepared by Fe(OD)3 → α-FeOOD conversion which was investigated by x-ray powder, TG, DTA and electron microscope techniques. The endothermic dehydration DTA peak of α-FeOOD occurs at a 10°C higher temperature than that of α-FeOOH (analogously prepared), the exothermic peak corresponding to the crystallization to Fe2O3 lies 5°C higher for α-FeOOD.
    Notes: Es wird eine Methode zur Darstellung von schwerem Eisenhydroxid vom Goethittyp, α-FeOOD, beschrieben. Die Umwandlung Fe(OD)3 → α-FeOOD wurde röntgenographisch, elektronenmikroskopisch, thermogravimetrisch und differentialthermoanalytisch untersucht. Im Vergleich zu unter analogen Bedingungen erzeugtem α-FeOOH liegt bei FeOOD der mit der Wasserabgabe verbundene endotherme Peak um 10°C höher, der durch die Kristallisation zu Fe2O3 verursachte exotherme Peak ist analog um 5°C verschoben.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
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