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  • 1
    Publication Date: 2019-07-13
    Description: An investigation was conducted to measure and understand the physical and mechanical effects that occur in boron fibers during and after thermal treatment in a controlled oxygen argon gaseous mixture. Of principal concern was the optimization of this treatment as a secondary processing method for significantly improving fiber tensile strength. Strengthening was accomplished by an oxidation induced axial contraction of the fiber and a resulting axial compression of strength limiting flaws within the fiber's tungsten boride core. Various physical observations were used to develop mechanistic models for oxidation, contraction, and flow formation. Processing guidelines are discussed for possibly exceeding the 5.5 GN/sq m strength limit and also for achieving fiber strengthening during application of boron containing diffusion barrier coatings.
    Keywords: COMPOSITE MATERIALS
    Type: NASA-TM-82599 , E-846 , Ann. Conf. on Composites and Advanced Mater.; Jan 18, 1981 - Jan 22, 1981; Merritt Island, FL; United States
    Format: application/pdf
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  • 2
    Publication Date: 2019-07-13
    Description: An investigation of the physical and mechanical effects of thermal treatment in a controlled oxygen-argon atmosphere on boron fibers is reported, with attention to the optimization of such treatment as a secondary processing method for improvement of fiber strength. The strengthening mechanism is comprised of an oxidation-induced axial contraction of the fiber, accompanied by axial compression of strength-limiting flaws within the fiber's tungsten boride core. It was found that after an oxidation contraction of 0.3% near 900 C, and a slight surface etch near 100 C, the average tensile strength of 203-micron fibers increased from 500 to 800 ksi. Various physical observations are used to develop mechanistic models of oxidation, contraction, and the formation of new flaws in the boron sheath at contractions greater than 0.3%.
    Keywords: COMPOSITE MATERIALS
    Type: Annual Conference on Composites and Advanced Ceramic Materials; Jan 18, 1981 - Jan 22, 1981; Merritt Island, FL
    Format: text
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