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  • AERODYNAMICS  (448)
  • Analytical Chemistry and Spectroscopy  (316)
  • GENERAL
  • 1975-1979  (764)
  • 1955-1959  (31)
  • 1
    Electronic Resource
    Electronic Resource
    La résonance magnétique du 77Se dans des composés organiques (1976)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 8 (1976), S. 354-356 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: 77Se n.m.r. spectra of twenty-six organoselenium compounds, including some with an endocyclic selenium atom, have been recorded. Our measurements complete the scale of chemical shifts previously established by McFarlane. It seems difficult to define a range of chemical shifts which is characteristic of the valency state of selenium or of its endo- or exocyclic position. Some results are discussed qualitatively. In the case of selenolo[2,3-b]thiophene, evidence has been obtained for a 4J[Se, H] coupling across the sulphur atom.
    Notes: La résonance magnétique du 77Se a été observée dans vingt-six composés organiques dont certains contiennent un atome de sélénium endocyclique. Nous avons pu ainsi compléter l'échelle de déplacements chimiques établie par McFarlane. II apparaît difficile de définir une gamme de déplacement chimique du 77Se caractéristique de son état de valence ou de sa position endo- ou exocyclique. Certains résultats sont discutés qualitativement. Dans le cas du sélénolo [2,3-b]thiophène, des arguments en faveur d'un couplage 4J(Se, H) à travers l'atome de soufre ont été découverts.
    Additional Material: 4 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270080706
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  • 2
    Electronic Resource
    Electronic Resource
    A soft X-ray spectrometer for the study of plutonium and plutonium-based materialsWork performed under the auspices of the US Department of Energy by Lawrence Livermore Laboratory, under contract number W-7405-ENG-48. (1978)
    New York, NY [u.a.] : Wiley-Blackwell
    X-Ray Spectrometry 7 (1978), S. 160-163 
    Details
    ISSN: 0049-8246
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: A low-energy spectrometer for the X-ray analysis of plutonium and plutonium-containing materials has been built. We use ultra-thin window to maintain different pressures and contamination level in the spectrometers's sample and crystal chambers. Ultra-thin windows are also used on the X-ray tube and detector. Methods have been developed by which the spectrometer can analyze both metal and loose-powder samples. Representative calibration spectra are presented for the fluorine band in polyfluoroethylene, the oxygen band in α-Al2 O3, and the carbon band in graphite. Experimental spectra are presented for the fluorine band in PuF3 and for the oxygen ban in PuO2.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/xrs.1300070310
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  • 3
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    Aerodynamic characteristics in ground proximity (1976)
    In:  CASI
    Details
    Publication Date: 2016-06-07
    Description: Results from recent investigations in the Langley V/STOL tunnel of an externally blown flap and an upper surface blown flap configuration in ground proximity are presented. Comparisons of longitudinal aerodynamic characteristics indicate that in ground proximity, drag is reduced for both configurations, but changes in lift are configuration dependent. Steady state analyses of the landing approach indicate an increase in flight path angle for both configurations in ground proximity because of the drag reduction. Dynamic analyses with a fixed-base simulator indicate that the resultant flight path during landing approach is dependent on the initial flight path angle and the control technique used.
    Keywords: AERODYNAMICS
    Type: Powered-Lift Aerodyn. and Acoustics; p 145-158
    Format: application/pdf
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    NASA TECHNICAL REPORTS
  • 4
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    Steady and unsteady transonic flow (1978)
    In:  Other Sources
    Details
    Publication Date: 2019-07-13
    Description: An investigation of the transonic flow over a circular arc airfoil was conducted to obtain basic information for turbulence modeling of shock-induced separated flows and to verify numerical computer codes which are being developed to simulate such flows. The investigation included the employment of a laser velocimeter to obtain data concerning the mean velocity, the shear stress, and the turbulent kinetic energy profiles in the flowfield downstream of the airfoil midchord where the flow features are more complex. Depending on the free-stream Mach number, the flowfield developed was either steady with shock-wave-induced separation extending from the foot of the shock wave to beyond the trailing edge or unsteady with a periodic motion also undergoing shock-induced separation. The experimental data were compared with the results of numerical simulations in which a computer code was employed that solved the time-dependent Reynolds' averaged compressible Navier-Stokes equations.
    Keywords: AERODYNAMICS
    Type: AIAA PAPER 78-160 , Aerospace Sciences Meeting; Jan 16, 1978 - Jan 18, 1978; Huntsville, AL
    Format: text
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    NASA TECHNICAL REPORTS
  • 5
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    An experimental and computational investigation of the flow field about a transonic airfoil in supercritical flow with turbulent boundary-layer separation (1976)
    In:  Other Sources
    Details
    Publication Date: 2019-07-13
    Description: A combined experimental and computational research program for testing and guiding turbulence modeling within regions of separation induced by shock waves incident on turbulent boundary layers is described. Specifically, studies are made of the separated flow over the rear portion of an 18%-thick circular-arc airfoil at zero angle of attack in high Reynolds number supercritical flow. The measurements include distributions of surface static pressure and local skin friction. The instruments employed include high-frequency response pressure cells and a large array of surface hot-wire skin-friction gages. Computations at the experimental flow conditions are made using time-dependent solutions of ensemble-averaged Navier-Stokes equations, plus additional equations for the turbulence modeling.
    Keywords: AERODYNAMICS
    Type: ICAS PAPER 76-15 , Congress; Oct 03, 1976 - Oct 08, 1976; Ottawa; Canada
    Format: text
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    NASA TECHNICAL REPORTS
  • 6
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    Aerodynamic drag reduction tests on a full-scale tractor-trailer combination and a representative box-shaped ground vehicle (1975)
    In:  Other Sources
    Details
    Publication Date: 2019-07-13
    Keywords: AERODYNAMICS
    Type: SAE PAPER 750703 , West Coast Meeting; Aug 11, 1975 - Aug 14, 1975; Seattle, WA
    Format: text
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    NASA TECHNICAL REPORTS
  • 7
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    On turbulence modeling for unsteady transonic flows (1979)
    In:  Other Sources
    Details
    Publication Date: 2019-07-13
    Description: A detailed examination of the turbulent field in an unsteady transonic flow undergoing shock-induced separation is conducted. Ensemble-averaged mean and fluctuating velocities, obtained from conditionally sampled laser velocimeter data, are described and analyzed to assess the applicability of modeling concepts usually employed in steady-flow problems. Some comparisons with computations employing the Reynolds averaged Navier-Stokes equations with a mixing length turbulence model are then presented to illustrate the status of current predictive capabilities. The results appear to imply that turbulence models developed for steady flows apply and that the model need not reflect all the fine details of the turbulent structure but rather account in an approximate way for the production and destruction of the turbulence.
    Keywords: AERODYNAMICS
    Type: AIAA PAPER 79-0071 , American Institute of Aeronautics and Astronautics, Aerospace Sciences Meeting; Jan 15, 1979 - Jan 17, 1979; New Orleans, LA
    Format: text
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    NASA TECHNICAL REPORTS
  • 8
    Electronic Resource
    Electronic Resource
    Identification of 4,6-O-(1-carboxyethylidene)-D-galactose by combined gas chromatogrphy mass spectrometry (1978)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 5 (1978), S. 671-673 
    Details
    ISSN: 0306-042X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Combined gas chromatography mass spectrometry was used to separate and identify a carrageenan component suspected of being the acid ketal 4,6-O-(1-carboxyethylidene)-D-galactose. The mass spectral fragmentation pattern is presented as evidence for the presence of this component in the carrageenan from Petrocelis middendorfii (P. francisana).
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200051207
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  • 9
    Electronic Resource
    Electronic Resource
    The effect of crystal size on the bioavailability of benoxaprofen: Studies utilizing deuterium labeled drug (1979)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 6 (1979), S. 173-178 
    Details
    ISSN: 0306-042X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A study of the effect of crystal size on the bioavailability of benoxaprofen, 2-[4-chlorophenyl]-α-methyl-5-benzoxazoleacetic acid, in man is reported. The technique utilized comparison of either the plasma concentrations or urine levels, resulting from administration of deuterium labeled (2H7) drug in solution coadministered with a test capsule formulation. Drug concentrations were determined by gas chromatography, and the ratio of labeled to unlabeled drug was obtained by gas chromatography mass spectrometry. Measurements following coadministration of labeled and unlabeled drug in solution established the absence of an isotope effect due to the presence of deuterium. The dry formulations consisted of either a 3.17-100 micron fraction (mean = 18.5 microns) or a 32-1000 micron fraction (mean = 610 microns) formulated with starch powder. The results in three subjects indicate an almost complete availability (0.95-0.98) of the small crystals as measured by comparison of either area under the plasma level curves or urine excretion (0.94-0.97) of labeled versus unlabeled drug measured to 168 hours. The larger crystals exhibited a lower availability as shown by plasma levels (0.41-0.46) or urine recovery (0.39-0.43). A higher dose of the large crystal formulation resulted in decreased relative availability with a fourfold dose dropping availability to 0.22 in a single subject.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200060409
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  • 10
    Electronic Resource
    Electronic Resource
    Gas phase carboxylate anions from p-nitrobenzyl esters of fatty acids (1978)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 5 (1978), S. 380-381 
    Details
    ISSN: 0306-042X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Gas phase carboxylate anions have been efficiently generated from the p-nitrobenzyl esters of nine fatty acids ranging in size from C6 to C22. The process involves the dissociative resonance capture of 2.9 eV electrons by the derivatives. The procedure is specific and gives the carboxylate anions as the base peak in all but two of the derivatives. The technique gives extremely simple spectra, with little additional fragmentation and no rearrangement ions.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200050603
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