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  • Gas chromatography  (2)
  • Amphotericin B  (1)
  • Boiler feed water and steam condensates  (1)
  • 1
    Electronic Resource
    Electronic Resource
    Epididymal histoplasmosis diagnosed by isolation ofHistoplasma capsulatum from semen (1995)
    Springer
    Mycopathologia 131 (1995), S. 173-177 
    Details
    ISSN: 1573-0832
    Keywords: Amphotericin B ; Epididymal histoplasmosis ; Histoplasma capsulatum ; Semen culture
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology , Medicine
    Notes: Abstract An autochthonous case of epididymal histoplasmosis masquerading as tuberculosis in a 55-year-old male patient is reported from India. It was diagnosed by culture ofHistoplasma capsulatum from semen and by demonstration of the fungus upon re-examination of epididymal biopsy sections previously misinterpreted as tuberculous granuloma. The patient's main complaints were painful epididymal swelling, occasional fever and cough. He was treated successfully by excision of epididymis and vas deferens combined with amphotericin B therapy. This is believed to be the first case of epididymal histoplasmosis to be reported outside the American continent and the fourth of its type reported in the English literature. The case is also noteworthy in thatH. capsulatum was isolated for the first time from semen, and it underlines the importance of mycological culture of semen specimens for diagnosis of genitourinary infections of obscure etiology.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01102897
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  • 2
    Electronic Resource
    Electronic Resource
    Gas chromatographic determination of residual hydrazine and morpholine in boiler feed water and steam condensates (1994)
    Springer
    Chromatographia 38 (1994), S. 456-460 
    Details
    ISSN: 1612-1112
    Keywords: Gas chromatography ; Morpholine ; Hydrazine ; Boiler feed water and steam condensates
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary Hydrazine, an oxygen scavenger in boiler water, was derivatised to the corresponding acetone azine and determined at the ng ml−1 level by gas chromatography. Morpholine, a corrosion inhibitor used in steam boilers, was estimated either directly (if 〉2.0 μg ml−1) or by quantitative preconcentration (0.1 ng – 2.0 μg ml−1). To obtain symmetrical peaks for these amines, the column packing was coated with KOH. Use of a nitrogen-specific detector improved accuracy of estimation of hydrazine and morpholine, giving a RSD of 1.9–3.6%. Chromatographic analysis of these amines in boiler feed water and steam condensate samples collected from boilers servicing a petroleum refinery is described. Environmental safety regulations calls for monitoring of hydrazine and the methods developed can easily be adapted for this purpose.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02269836
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  • 3
    Electronic Resource
    Electronic Resource
    A simple gas chromatographic method for the analysis of oxygenates in gasoline (1995)
    Springer
    Chromatographia 40 (1995), S. 607-610 
    Details
    ISSN: 1612-1112
    Keywords: Gas chromatography ; Packed column separations ; C1−C4 alcohols ; Ethers ; Gasoline
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary A number of oxygenated compounds such as C1−C4 alcohols, methyl tert-butyl ether (MTBE), and tertamyl methyl ether (TAME) are increasingly being used in gasoline as octane boosters and to reduce vehicular emissions. Monitoring of individual oxygenates in gasoline is important for quality control and regulatory purpose. Although, several analytical methods based on gas chromatography have been reported, a need was still felt to develop a simple and cost effective method of analysis. In this paper, a packed column gas chromatographic method is described for the analysis of C1−C4 alcohols, MTBE and TAME over a wide concentration range (2–20% V/V) in gasoline. The method involves determination of alcohols and ethers separately on two different columns. The alcohols are determined on a 20 ft column packed with poly(ethylene glycol) 400 as a stationary phase while the ethers are analysed on a 20 ft OPN-Poracil C column. The analysis of alcohols on poly(ethylene glycol) 400 column also provides data on aromatic components of gasoline.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02290276
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