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Thermostable persilylated polar glass capillary columns by the ammonia-etching method (1981)

Traitler, H. ; Prévôt, A.

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 4 (1981), S. 433-436

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ISSN: 0935-6304

Keywords: Gas chromatography ; Capillary, glass ; Persilylation ; Polar phases ; Ammonia etching ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Static ammonia etching has been used to effect regular surface roughening of glass capillaries. Following such treatment, polar phases could be coated after persilylation with varioussilylation agents such as hexamethyl-, tetramethyldiphenyl-, and tetra- phenyldimethyldisilazane, respectively. This method produces columns of high thermostability, which is limited only by the maximum applicable temperature for the phase itself.

Additional Material: 5 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/jhrc.1240040902

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