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Solid-state NMR study of a series of aminophosphonic acids (1989)

Harris, Robin K. ; Merwin, Lawrence H. ; Hägele, Gerhard

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 27 (1989), S. 470-475

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ISSN: 0749-1581

Keywords: Solid-state NMR ; Aminophosphonic acids ; Crystallography ; Shielding tensors ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: High-resolution 31P, 15N and 13C NMR spectra have been obtained for nine solid aminophosphonic acids under conditions of high-power decoupling, cross-polarization and magic-angle spinning. The NMR evidence shows that the asymmetric unit is a single molecule in all cases, which is consistent with the available diffraction studies. Phosphorus-31 shielding tensor components determined from static and slow-spinning MAS spectra are given for a number of the compounds.

Additional Material: 5 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260270509

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