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  • 1
    Electronic Resource
    Electronic Resource
    The Syntheses and Molecular Structure of a Branched Oligosilyl Anion with a Record of Nine Silicon Atoms and of the First Branched Oligosilyl Dianion (2000)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 2000 (2000), S. 1091-1095 
    Details
    ISSN: 1434-1948
    Keywords: Silicon ; Silyl anions ; Lithium ; Silanes ; Polysilyl dianions ; α,ω-Dilithiooligosilanes ; Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: (Me3Si)3Si(Me2Si)2(Me3Si)2SiLi (1) and LiSi(Me3Si)2(Me2Si)2Si(Me3Si)2Li (2) were synthesized by the reaction of (Me3Si)3Si(Me2Si)2Si(Me3Si)3 in THF with one or two mol-equivalents, respectively, of MeLi. Both 1 and 2 were characterized spectroscopically and by trapping reactions, and 1 also by X-ray crystallography.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
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    Paper (German National Licenses)
  • 2
    Electronic Resource
    Electronic Resource
    Synthesis of 2-Fluoro Analogues of Frontalin (2000)
    Weinheim : Wiley-Blackwell
    Liebigs Annalen 2000 (2000), S. 1387-1389 
    Details
    ISSN: 1434-193X
    Keywords: Natural products ; Epoxidations ; Asymmetric synthesis ; Fluorine ; Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: ---The synthesis of enantiomerically and diastereomerically pure (-)-(1R,2R,5R)- and (-)-(1R,2S,5R)-2-fluoro frontalin (7) starting from (+)-(1S)-menthyl-(R)-toluene-4-sulfinate, methylmagnesium bromide, methyl fluoroacetate, 4-pentenyl bromide and diazomethane is described. The absolute stereochemistry was unambiguously determined by X-ray analysis of (+)-(1S,2R,5S,RS)-5, an intermediate in the synthesis of the enantiomeric (+)-(1S,2R,5S)-2-fluoro frontalin (7).
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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    Paper (German National Licenses)
  • 3
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    Seismic imaging of a convergent continental margin and plateau in the central Andes (Andean Continental Research Project 1996 (ANCORP'96)) (2003)
    In:  Journal of Geophysical Research
    Details
    Publication Date: 2020-02-12
    Description: A 400-km-long seismic reflection profile (Andean Continental Research Project 1996 (ANCORP'96)) and integrated geophysical experiments (wide-angle seismology, passive seismology, gravity, and magnetotelluric depth sounding) across the central Andes (21°S) observed subduction of the Nazca plate under the South American continent. An east dipping reflector (Nazca Reflector) is linked to the down going oceanic crust and shows increasing downdip intensity before gradual breakdown below 80 km. We interpret parts of the Nazca Reflector as a fluid trap located at the front of recent hydration and shearing of the mantle, the fluids being supplied by dehydration of the oceanic plate. Patches of bright (Quebrada Blanca Bright Spot) to more diffuse reflectivity underlie the plateau domain at 15–30 km depth. This reflectivity is associated with a low-velocity zone, P to S wave conversions, the upper limits of high conductivity and high Vp/Vs ratios, and to the occurrence of Neogene volcanic rocks at surface. We interpret this feature as evidence of widespread partial melting of the plateau crust causing decoupling of the upper and lower crust during Neogene shortening and plateau growth. The imaging properties of the continental Moho beneath the Andes indicate a broad transitional character of the crust-mantle boundary owing to active processes like hydration of mantle rocks (in the cooler parts of the plate margin system), magmatic underplating and intraplating under and into the lowermost crust, mechanical instability at Moho, etc. Hence all first-order features appear to be related to fluid-assisted processes in a subduction setting
    Keywords: 550 - Earth sciences
    Type: info:eu-repo/semantics/article
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