ISSN:
0749-1581
Keywords:
13C,31P NMR correlation
;
HMQC
;
Triple resonance
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
Three different experimental techniques are compared to find the most efficient protocol for 2D 13C, 31P correlation spectroscopy. It is shown that the best signal-to-noise ratio is given by the polarization transfer experiment for 31P detection and by the HMQC experiment for 13C detection. Applications of these techniques for 13C,31P correlation of β-nicotinamide adenine dinucleotide (NAD+) and a mixture of three different mononucleotides are described.
Additional Material:
5 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/mrc.1260300704
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