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Cathodic Reduction of 1-Nitroalkenes to Oximes and Primary Amines (1991)

Wessling, Michael ; Schäfer, Hans J.

Weinheim : Wiley-Blackwell

Berichte der deutschen chemischen Gesellschaft 124 (1991), S. 2303-2306

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ISSN: 0009-2940

Keywords: Electrochemistry ; 1-Nitroalkenes, reduction of ; Oximes ; Amines ; Chemistry ; Inorganic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: 1-Nitroalkenes are reduced in high yields at -0.3 to -0.5 V (vs. SCE) at a mercury or graphite cathode to oximes. At higher cathodic reduction potentials (- 1.1 V) primary amines are selectively obtained in fair yields. Nitroalkadienes are selectively reduced at the double bond conjugated with the nitro group to either the oxime or amine.

Additional Material: 4 Tab.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/cber.19911241024

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