ISSN:
1573-9171
Keywords:
[dimethy(diethylamino)silyl]- and [methyl-bis(diethylamino)silyl]methylmagnesium chlorides
;
(methylchlorosilyl)methyldichlorophosphines
;
NMR spectroscopy
Source:
Springer Online Journal Archives 1860-2000
Topics:
Chemistry and Pharmacology
Notes:
Abstract (Methylchlorosilyl)methyldichlorophosphines have been synthesized by the reaction of [dimethy(diethylamino)silyl]- or [methyl-bis(diethylamino)silyl]methylmagnesium chlorides with PCl3 in ether at −40÷−20 °C and subsequent treatment of the reaction mixture with dry HCl. The structures of the compounds thus obtained have been studied by31P,1H, and13C NMR spectroscopy.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF00698970
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