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  • 1
    ISSN: 1612-1112
    Keywords: Capillary gas chromatography ; Natural products ; Citrus analysis ; Pre-separation by gel-permeation ; Pre-column
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Die Gaschromatographie von Naturstoffen wird durch nicht-flüchtige Anteile sehr erschwert. Störungen erfolgen durch Krackung und Katalysatorwirkung im Einspritzblock, Geisterpeaks und Grundlinienversatz. Mittels einer einfachen Gelchromatographie-Vortrennung wird eine Verbesserung der Citrusölanalytik beschrieben. Werden die höhermolekularen Stoffe nicht benötigt, kann man diese durch Verwendung einer Vorsäule am Gaschromatographen ausschalten. Ein einfacher Umbau am GC Gerät wird angegeben.
    Notes: Summary GC separation of natural products is upset by nonvolatile compounds. The problems arise from thermal and catalytic cracking in the injector, from ghost peaks and base line drift. A treatment is shown for obtaining an improvement in citrus analysis by using simple gelpermeation chromatography for pre-separation. A second method describes the separation of the high relative molecular mass compounds with a pre-column GC-equipment. A simple conversion is demonstrated for this modification of GC apparatus.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 29 (1983), S. 677-685 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Wall-to-bed heat transfer coefficients in three-phase fluidized beds with glass beads and clyindrical γ-alumina particles were determined experimentally. In the present study, the relative increase in heat transfer coefficient was found equal to the relative decrease in liquid holdup in three-phase fluidized beds. Modified Stanton number has been correlated with modified Reynolds number.
    Additional Material: 11 Ill.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 31 (1985), S. 1504-1509 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Liquid holdups and wall-to-bed heat transfer coefficients in three-phase fluidized beds with glass beads and cylindrical γ-alumina particles were determined experimentally. It was found that the product of heat transfer coefficient and liquid holdup in three-phase fludized beds is equal to that in corresponding liquid-solid fluidized beds. A generalized correlation equation for heat transfer coefficients in both liquid-solid and three-phase fluidized beds was proposed based on the above relationship.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
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