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  • Cambridge University Press  (1)
  • Woods Hole Oceanographic Institution  (1)
  • 1
    Publication Date: 2022-05-26
    Description: We have developd a computer controlled system to measure the calcium carbonate content of sediment samples. A menu driven program controls the analysis of each sample. The system first communicates with a Mettler digital balance to record the weights of the 40 samples which must be loaded into each run. The sample boats are next loaded into the sample carousel which is then sealed from the atmosphere. The system is first pumped down to a vacuum of 0.04 torr. The valve to the pump closes and the stepping motor turns the carousel, moving a sample boat over the delivery slot and dropping the sample into 80°C 100% phosphoric acid under vigorous spinning action. During the reaction, carbonate is evolved into H2O and CO2 and the resulting pressure change within the closed system is measured by a pressure transducer and recorded into memory next to the sample identification and sample weight. The system is pumped once again to 0.04 torr and the process continues until all 40 samples have been analyzed. The data can then be uploaded and converted to percent carbonate values using a regression line produced from multiple analyses of varying weights of a 100% carbonate standard. Precision of the system, based upon 120 replicate analysis ranges from 0.49% to 0.88%.
    Description: Funding was provided by the National Science Foundation through Grant Nos. OCE 85-11014 and OCE 88-13307.
    Keywords: Carbonate ; Automated ; Sediments
    Repository Name: Woods Hole Open Access Server
    Type: Technical Report
    Format: 1698741 bytes
    Format: application/pdf
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  • 2
    Publication Date: 1996-07-01
    Description: Deep-sea sediments recovered from six sites visited during the International Arctic Ocean Expedition of 1991 were examined to determine sedimentation rates in the eastern Arctic Ocean basin. The dearth of age-diagnostic biogenic material in these sediments precludes the application of biostratigraphic methods, but ages can be deduced using paleomagnetism, in conjunction with measurements of radiocarbon and carbonate concentration. Although no one of these techniques gives an unambiguous determination of age, the interpretation most consistent with these diverse data implies that sedimentation rates in the eastern Arctic are, in general, a few centimeters per thousand years. Such estimates of sedimentation rate are an order of magnitude greater than those previously determined from many sediment cores taken from the Canada Basin. However, one site examined on the Morris Jesup Rise shows a relatively low rate of sediment accumulation (less than 0.6 cm/103 yr) suggesting that, although higher than in the Canada Basin, sedimentation rates in the eastern Arctic can be highly variable.
    Print ISSN: 0033-5894
    Electronic ISSN: 1096-0287
    Topics: Geography , Geosciences
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