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  • Wiley-Blackwell  (3)
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  • 1
    Electronic Resource
    Electronic Resource
    Structural investigations on the inner core region of lipopolysaccharides from Salmonella minnesota rough mutantsSome of the results were presented at the 5th International Symposium on Mass Spectrometry in Life Science, Ghent/Belgium, 1984. Dedicated to Dr. O. Lüderitz on the occasion of his 65th birthday (1985)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 12 (1985), S. 602-609 
    Details
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The structure of the inner core region (L-glycero-D-mannoheptose/2-keto-3-deoxy-D-mannooctulosonic acid region) of lipopolysaccharides from Salmonella minnesota rough mutants was investigated. Using conventional methods (neutral sugar analysis, Smith degradation and methylation analysis) combined with gas chromatography/mass spectrometry (GC/MS) of higher oligosaccharides (up to tetrasaccharide), the linkages of the core sugars of lipopolysaccharides from S. minnesota rough mutants, strains R4 (Rd2P-), R7 (Rd1P-) and R5 (RcP-) were determined as: with R representing H in R4, L-glycero-D-mannoheptopyranosyl in R7, and D-glucopyranosyl-(1→3)-L-glycero-D-mannoheptopyranosyl in R5, respectively. In addition, it is shown that heterogeneity within the neutral sugar part of these lipopolysaccharides is low.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200121007
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  • 2
    Electronic Resource
    Electronic Resource
    Die Elementarzelle und Raumgruppe von Strontiumjodid (1967)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 354 (1967), S. 23-26 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: From Buerger precession photographs of SrJ2 (MoKα radiation) the lattice dimensions a = 15.22, b = 8.22, c = 7.90 Å and the space group Pbca are derived. According to the calculated and measured density (ϱc = 4.59 g/cm3, ϱm = 4.549 g/cm3) the orthorhombic unit cell contains 8 formula units SrJ2. EuJ2 and SrJ2 are not isostructural, but there are close material relations between their unit cells.
    Notes: Aus BUERGER-Präzessionsaufnahmen von SrJ2 (MoKα-Strahlung) wurden die Gitterkonstanten a = 15,22, b = 8,22 und c = 7,90 Å sowie die Raumgruppe Pbca abgeleitet. Die rhombische Elementarzelle enthält gemäß Dichtevergleich (ϱber = 4,59 g/cm3, ϱexp = 4,549 g/cm3) 8 Formeleinheiten SrJ2. EuJ2 und SrJ2 sind nicht isotyp; es bestehen aber enge Beziehungen zwischen den Abmessungen der Elementarzellen.
    Additional Material: 1 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19673540106
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  • 3
    Electronic Resource
    Electronic Resource
    Die Kristallstruktur von Strontiumjodid SrJ2 (1969)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 368 (1969), S. 62-72 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: The crystal structure of SrI2 was solved by means of a three-dimensional PATTERSON synthesis and refined by the method of least squares to a reliability index of 8.6%. The most striking feature of this structure, which represents a new structure type, is the sevenfold coordination of I--ions about the cation Sr2+. Very similar coordination polyhedra were found in the recently solved structures of CeSI and EuI2 (monoclinic modification), but only the former crystallizes isostructural with SrI2; the latter shows another connection principle of the polyhedra.
    Notes: Die Kristallstruktur von SrJ2 wurde mit Hilfe einer dreidimensionalen PATTERSON-Synthese gelöst und nach der Methode der kleinsten Quadrate bis auf einen Zuverlässigkeitsindex von 8,6% verfeinert. Das auffälligste Merkmal dieser Struktur, die einen neuen Strukturtyp verkörpert, ist die siebenfache Koordination von J--Ionen um das Kation Sr2+. Recht ähnliche Koordinationspolyeder wurden in den kürzlich aufgeklärten Strukturen von CeSJ und EuJ2 (monokline Form) gefunden, aber nur die erstgenannte Verbindung kristallisiert isotyp zu SrJ2; die letztere weist ein anderes Verknüpfungsprinzip der Polyeder auf.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19693680110
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