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  • 1
    Electronic Resource
    Electronic Resource
    Real-time measurement of RFR energy distribution in the macaca mulatta head (1980)
    New York, NY [u.a.] : Wiley-Blackwell
    Bioelectromagnetics 1 (1980), S. 21-34 
    Details
    ISSN: 0197-8462
    Keywords: radiofrequency radiation ; microwaves ; rhesus monkey dosimetry ; microwave dosimetry ; cranial structures ; Life and Medical Sciences ; Occupational Health and Environmental Toxicology
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Biology , Physics
    Notes: Temperature increases due to absorption of 1.2 GHz, CW, 70 mW/cm2, radio frequency (RF) energy, were measured in 3.3-cm-radius homogeneous muscle-equivalent spheres, M. mulatta cadaver heads (both detached from and attached to the body) and living, anesthetized M. mulatta heads. Temperatures were measured with a Vitek, Model 101 Electrothermia Monitor and temperature distributions were compared to theoretical predictions from a thermal-response model of a simulated cranial structure. The results show that the thermal response model accurately predicts the temperature distribution in muscle-equivalent spheres, the distribution of temperature in detached M. mulatta heads when exposed from the back of the head, and the distribution of temperature in attached M. mulatta cadaver heads for animals oriented with body parallel to the H-field. The temperature distribution in the detached M. mulatta heads varies markedly with exposure orientation, ie, facing forward, backward, or to the side. The orientation of the M. mulatta cadaver body significantly affects the temperature distribution in the head - with H-field orientation showing high, nonuniform values, and E-field orientation showing low, uniform values. In live animals blood flow produces a significant short-term effect on the temperature distribution in the midbrain, but not the cortex. Midbrain temperatures are both significantly higher and lower than the comparable cadaver measurements, depending on location.
    Additional Material: 10 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bem.2250010103
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  • 2
    Electronic Resource
    Electronic Resource
    Ceric-initiated polymerization onto polyacrylonitrile with carbohydrate end groups. Graft versus block copolymer formation (1983)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Chemistry Edition 21 (1983), S. 2095-2100 
    Details
    ISSN: 0360-6376
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Starch-g-polyacrylonitrile (starch-g-PAN) copolymers were prepared by ceric ammonium nitrate initiation, and the major portion of the starch in these graft copolymers was then removed by acid hydrolysis to yield PAN with oligosaccharide end groups. Although these PAN-oligosaccharide samples reacted with methyl methacrylate in the presence of ceric ammonium nitrate, the resulting products were largely graft copolymers rather than the expected PAN-poly(methyl methacrylate) (PMMA) block copolymers. The following evidence is presented for a PAN-g-PMMA structure: (i) PAN without oligosaccharide end groups also produced a copolymer with methyl methacrylate under our reaction conditions. (ii) Starch-g-PAN (51 or 37% add-on) was a less reactive substrate toward ceric-initiated polymerization than PAN with oligosaccharide end groups. (iii) Low-add-on (18%) starch-g-PAN reacted with methyl methacrylate to give a final graft copolymer in which a large percentage of PMMA was grafted to the PAN component rather than to starch.
    Additional Material: 2 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1983.170210719
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  • 3
    Electronic Resource
    Electronic Resource
    Polymerization of alkyl acrylates and alkyl methacrylates with starch (1980)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 25 (1980), S. 2285-2294 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: A series of C4-C12 alkyl acrylates and methacrylates was polymerized with starch by irradiating starch-monomer mixtures with 60Co. Homopolymers were extracted with cyclohexane. The amounts of insoluble versus soluble synthetic polymer in polymerization run with alkyl acrylates varied less with the chain length of the alkyl substuent than in the polymerizations run with alkyl acrylates varied less with the chain length of the alkyl substituent than in the polymerizations run with alkyl methacrylates; and the poly(alkyl acrylate) contents of cyclohexane-insoluble fractions were all in the 38-45% range. Synthetic polymer contents of the products from butyl, hexyl, and decyl methacrylates were also close to this range. Octyl and lauryl methacrylate, however, gave high conversions to cyclohexane-soluble poly(alkyl methacrylate) along with little or no unextractable synthetic polymer in the starch-containing fractions. Poly(lauryl methacrylate) could be rendered insoluble by incorporating a small amount of tetramethylene glycol dimethacrylate in the polymerization mixture. In a series of polymerizations run with hexyl acrylate and hexyl methacrylate, lower irradiation doses led to more cyclohexane-soluble polymer and less synthetic polymer in the starch-containing fractions. Enzymatic digestion of starch-soluble polymer and less synthetic polymer in the starch-containing fractions. Enzymatic digestion of starch-containing polymers gave synthetic polymer fractions that were largely insoluble in cyclohexane. Crosslinking is, therefore, probably taking place during these polymerizations; however, we could not eliminate the possibility that reduced solubility was caused by small amounts of residual carbohydrate in these polymer fractions. Ceric ammonium nitrate-initiated polymerizations of butyl acrylate, hexyl acrylate, and butyl methacrylate with starch gave cyclohexane-insoluble polymers that contained 33-39% synthetic polymer. The higher alkyl acrylates and methacrylates produced little or no polymer under these conditions. Starch-containing fractions were tested as absorbents for hydrocarbons. Products prepared from decyl acrylate and lauryl acryle acrylate absorbed about 9 g of isooctane per 1 g of polymer, whereas the lowrer alkyl monomers gave polymers with lower absorbency.
    Additional Material: 5 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1980.070251015
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  • 4
    Electronic Resource
    Electronic Resource
    Graft polymerizations of acrylonitrile and methyl acrylate onto starch and cellulose at different stirring speeds (1984)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 29 (1984), S. 4449-4453 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Additional Material: 2 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1984.070291278
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  • 5
    Electronic Resource
    Electronic Resource
    Graft polymerization of acrylonitrile and methyl acrylate onto hemicellulose (1982)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 27 (1982), S. 4239-4250 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Graft polymerizations of acrylonitrile onto both a commercial larchwood hemicellulose and a purified (low lignin) wheat straw hemicellulose could be initiated by ceric ammonium nitrate. The resulting hemicellulose-g-polyacrylonitrile (PAN) copolymers were fractionated by extraction at room temperature with dimethylformamide and dimethylsulfoxide. Fractions were characterized by determining both the wt % PAN in each polymer fraction and the molecular weight of grafted PAN. Saponification of the PAN component of hemicellulose-g-PAN gave a water-dispersible graft copolymer with good thickening properties for water systems. An absorbent polymer, similar to the starch-based absorbents (Super Slurpers), was produced when saponified hemicellulose-g-PAN was isolated by methanol precipitation and then dried. Larchwood hemicellulose was also graft-polymerized with methyl acrylate using ceric ammonium nitrate initiation, and the hemicellulose-g-poly(methyl acrylate) was extrusion-processed into a tough, leathery plastic. Although ceric ammonium nitrate could be used as an initiator for graft polymerizations onto low-lignin hemicelluloses, it was inert with crude wheat straw hemicellulose containing 11% lignin. The ferrous sulfate-hydrogen peroxide redox system was used to initiate graft polymerizations onto this high-lignin material, and properties of the resulting hemicellulose-g-poly(methyl acrylate) and saponified hemicellulose-g-PAN graft copolymers were evaluated.
    Additional Material: 2 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1982.070271115
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  • 6
    Electronic Resource
    Electronic Resource
    Saponified starch-g-polyacrylonitrile. Variables in the Ce+4 initiation of graft polymerization (1982)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 27 (1982), S. 2731-2737 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1982.070270740
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  • 7
    Electronic Resource
    Electronic Resource
    Graft copolymers of methyl acrylate onto bleached wood pulp: Preparation and extrudate properties (1983)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 28 (1983), S. 3003-3009 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1983.070280926
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  • 8
    Electronic Resource
    Electronic Resource
    Polysaccharide-g-polystyrene copolymers by persulfate initiation: Preparation and properties (1983)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 28 (1983), S. 2455-2461 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1983.070280730
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  • 9
    Electronic Resource
    Electronic Resource
    Hydrolysis of wheat straw hemicellulose with trifluoroacetic acid. Fermentation of xylose with Pachysolen tannophilus (1984)
    New York, NY [u.a.] : Wiley-Blackwell
    Biotechnology and Bioengineering 26 (1984), S. 1122-1125 
    Details
    ISSN: 0006-3592
    Keywords: Chemistry ; Biochemistry and Biotechnology
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Biology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Treatment of wheat straw with 1N trifluoroacetic acid (TFA) for 7 h at reflux temperature yielded 23% xylose based upon initial straw weight. This corresponds to about an 80% xylose yield based on the xylan content of the hemicellulose. The cellulose component of wheat straw was largely unaffected, as evidenced by low glucose yields. Decomposition of xylose by prolonged refluxing (23 h) was minimal in 1N TFA compared to 1N HCl. Treatment of wheat straw with refluxing 1N TFA converts about 10% of the lignin initially present in straw into water-soluble lignin fragments. Fermentation of the xylose-rich wheat straw hydrolyzate to ethanol with Pachysolen tannophilus was comparable to the fermentation of reagent grade xylose, indicating that furfural and toxic lignin by-products were not produced by 1N TFA in sufficient amounts to impair cell growth and ethanol production. Cellulase treatment of the wheat straw residue after TFA hydrolysis resulted in a 70-75% conversion of the cellulose into glucose.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bit.260260916
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