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Crystal and molecular structure of decahydroquinoline hydrobromide, and its relation to piperidine hydrobromide (1977)

Escobar, C. ; Garland, M. T. ; Wittke, O.

Springer

Journal of chemical crystallography 7 (1977), S. 69-79

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ISSN: 1572-8854

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract The structure of decahydroquinoline hydrobromide has been determined by the heavy-atom technique. This compound, C9H18NBr, crystallizes in the orthorhombic space groupPbcn (N ° 60), witha = 26.885(3),b = 9.952(1),c = 7.750(1) Å, andZ = 8. The structure was refined by block-diagonal least-squares methods to a finalR value of 0.086, including the hydrogen atoms located theoretically. Decahydroquinoline has a chair conformation. The molecules are held together by a network of hydrogen bonds of type N+−H...Br− along thec axis, and by van der Waals forces in the other directions. A comparative study with the structure of piperidine hydrobromide is given.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01369833

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