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  • 1
    Electronic Resource
    Electronic Resource
    A New Synthetic Route to Dialkylphosphinous Chlorides (1961)
    [s.l.] : Nature Publishing Group
    Nature 189 (1961), S. 916-916 
    Details
    ISSN: 1476-4687
    Source: Nature Archives 1869 - 2009
    Topics: Biology , Chemistry and Pharmacology , Medicine , Natural Sciences in General , Physics
    Notes: [Auszug] It has been found that alkylphosphonous dichlorides will form a complex with aluminium chloride and an alkyl halide in the same manner as does phosphorus trichloride5. Solution of this complex in an electron-donating solvent, for example diethyl phthalate (DEP), followed by reduction with powdered ...
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1038/189916a0
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    A New Synthetic Route to Alkylphosphonous Dichlorides (1960)
    [s.l.] : Nature Publishing Group
    Nature 188 (1960), S. 227-228 
    Details
    ISSN: 1476-4687
    Source: Nature Archives 1869 - 2009
    Topics: Biology , Chemistry and Pharmacology , Medicine , Natural Sciences in General , Physics
    Notes: [Auszug] The reactions are exothermic and proceed smoothly in a single flask. Yields of RPC12 from 90 to 55 per cent have been obtained repeatedly for R = CH3 to R = C5H11 Full details of the method and its application in high -activity synthesis of organophosphorus compounds labelled with radioactive ...
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1038/188227b0
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    Paper (German National Licenses)
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