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  • 1
    Publication Date: 2012-08-25
    Description: This is the second part of an article series where the mechanical and fracture mechanical properties of medium density fiberboard (MDF) were studied. While the first part of the series focused on internal bond strength and density profiles, this article discusses the fracture mechanical properties of the core layer. Fracture properties were studied with a wedge splitting setup. The critical stress intensity factors as well as the specific fracture energies were determined. Critical stress intensity factors were calculated from maximum splitting force and two-dimensional isotropic finite elements simulations of the specimen geometry. Size and shape of micro crack zone were measured with electronic laser speckle interferometry. The process zone length was approx. 5 mm. The specific fracture energy was determined to be 45.2 ± 14.4 J/m2 and the critical stress intensity factor was 0.11 ± 0.02 MPa.
    Electronic ISSN: 1996-1944
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Published by MDPI Publishing
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  • 2
    Publication Date: 2012-06-20
    Description: Internal bond strength testing is a widely used approach for testing quality traits of wood based panels. Generally, failure of internal bond specimens is due to adhesion and/or wood failure in the specimen. It has been reported that a composite product with a large variation in the vertical density profile fails in the center part of the board which is either the middle of the core layer or the transition zone between core layer and face layer. The density in the failure zone is typically 50% lower than the maximum density in the face layers. The aim of this study was to analyze the strain distribution in a specimen under tension perpendicular to the panel plane. The results showed that a high variety of strain magnitude occurred in the specimen. The strain is either aligned with the tension direction or a tension zone is built in one of the edge zones leading to failure. Vector graphics of the specimen show the problematic test setup of internal bond strength measurement. Strain spots in the edges lead to the assumption of an uneven stress distribution due to the momentum which results from non-perfect alignment or irregularities in the test setup.
    Electronic ISSN: 1996-1944
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Published by MDPI Publishing
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  • 3
    Publication Date: 2012-11-08
    Description: This paper is the third part of a study dealing with the mechanical and fracture mechanical characterization of Medium Density Fiberboards (MDF). In the first part, an analysis of internal bond strength testing was performed and in the second part MDF was analyzed by means of the wedge splitting experiment; this part deals with the double cantilever I beam test, which is designed for measuring the fracture energy as well as stress intensity factor in Mode I. For a comparison of isotropic and orthotropic material behavior, finite element modeling was performed. In addition to the calculation of fracture energy the stress intensity factor was analyzed by means of finite elements simulation and calculation. In order to analyze strain deformations and the process zone, electronic speckle pattern interferometry measurements were performed. The results revealed an elongated process zone and lower results for KIC if compared to the wedge splitting experiment. The Gf numbers are higher compared to the wedge splitting results and can be explained by the thicker process zone formed during the crack propagation. The process zone width on its part is influenced by the stiff reinforcements and yields a similar crack surface as with the internal bond test.
    Electronic ISSN: 1996-1944
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Published by MDPI Publishing
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  • 4
    Publication Date: 2006-07-01
    Description: The elastic modulus, hardness, and creep factor of wood cell walls in the interphase region of four different adhesive bonds were determined by nanoindentation. In comparison with reference cell walls unaffected by adhesive, interphase cell walls from melamine-urea-formaldehyde (MUF) and phenol-resorcinol-formaldehyde (PRF) adhesive bonds showed improved hardness and reduced creep, as well as improved elastic modulus in the case of MUF. In contrast, cell walls from the interphase region in polyvinylacetate (PVAc) and one-component polyurethane (PUR) bonds showed more creep, but lower elastic modulus and hardness than the reference. Considering the different cell-wall penetration behaviour of the adhesive polymers studied here, it is concluded that damage and loss of elastic modulus to surface cells occurring during the machining of wood is recovered in MUF and PRF bond lines, whereas damage of cell walls persists in PVAc and PUR bond lines.
    Print ISSN: 0018-3830
    Electronic ISSN: 1437-434X
    Topics: Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Published by De Gruyter
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  • 5
    Publication Date: 2008-01-01
    Description: Cross sections of wood adhesive bonds were studied by scanning thermal microscopy (SThM) with the aim of scrutinizing the distribution of adhesive in the bond line region. The distribution of thermal conductivity, as well as temperature in the bond line area, was measured on the surface by means of a nanofabricated thermal probe offering high spatial and thermal resolution. Both the thermal conductivity and the surface temperature measurements were found suitable to differentiate between materials in the bond region, i.e., adhesive, cell walls and embedding epoxy. Of the two SThM modes available, the surface temperature mode provided images with superior optical contrast. The results clearly demonstrate that the polyurethane adhesive did not cause changes of thermal properties in wood cell walls with adhesive contact. By contrast, cell walls adjacent to a phenol-resorcinol-formaldehyde adhesive showed distinctly changed thermal properties, which is attributed to the presence of adhesive in the wood cell wall.
    Print ISSN: 0018-3830
    Electronic ISSN: 1437-434X
    Topics: Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Published by De Gruyter
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  • 6
    Publication Date: 2013-02-01
    Description: Local variability in the thermal conductivity of the cell wall of beech wood fibers was studied by means of scanning thermal microscopy (SThM). In the cross section, the thermal conductivity of the secondary cell wall was essentially higher than that of the compound middle lamella (CML). In sections parallel to the cell axis, the overall conductivity of the S1 layer was lower than that of the secondary cell wall, but the S2 layer and the CML showed similar conductivities. This is attributed to the orientation of the cellulose microfibrils playing a key role in the observed anisotropies concerning the thermal conductivity. The deviating thermal conductivities on different sections are attributed to the depth effect of the thermal scanning. SThM proves to be a technique with considerable potential for wood research.
    Print ISSN: 0018-3830
    Electronic ISSN: 1437-434X
    Topics: Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Published by De Gruyter
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  • 7
    Publication Date: 2012-08-01
    Description: Spruce wood specimens were surface-silylated according to three different protocols in order to progressively reduce hydrophilicity and, consequently, adhesion to urea-formaldehyde (UF) glue. Compared to the untreated reference, the macroscopic adhesive strength was drastically reduced in silylated specimens. Specimens treated with the most effective silylation method in terms of reduction of hydrophilicity showed near zero adhesion to UF glue. Micromechanical characterisation by means of nanoindentation (NI, Berkovich-type probe) revealed that the wood cell wall stiffness and hardness was not significantly affected by silylation. Contrarily, NI experiments (conical indenter tip with 60° opening angle) performed directly at the interface between the wood cell wall and the adhesive showed significantly reduced hardness and reduced specific work of NI in silylated specimens. It is concluded that the measured correlation between reduced hydrophilicity in silylated specimens and the mechanical strength of the interface is due to reduced adhesion. This allows calculating the specific adhesive energy for the system wood cell wall–urea formaldehyde glue from the difference between the specific work of adhesion obtained from the unmodified reference and the most efficiently silylated specimen. The advantage of this new method lies in the position-resolved measurement of qualitative differences in adhesive energy directly at the interface. This is not feasible with macroscopic test methods, which also include effects of surface roughness, cellular adhesive penetration, or grain angle.
    Print ISSN: 0018-3830
    Electronic ISSN: 1437-434X
    Topics: Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Published by De Gruyter
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  • 8
    Publication Date: 2008-11-01
    Print ISSN: 0018-3830
    Electronic ISSN: 1437-434X
    Topics: Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Published by De Gruyter
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  • 9
    Publication Date: 2010-10-01
    Description: Three-part specimens were produced from Norway spruce wood (Picea abies Karst.) and bonded with the following adhesives: melamine-urea-formaldehyde (MUF), phenol-resorcinol-formaldehyde (PRF), and a two-component emulsion polymer isocyanate (EPI). The effect of alternating climate conditions on bond strength was studied by tensile tests. The specimens were exposed to a three-step ageing cycle lasting for 7 days [50°C/95% relative humidity (RH), -20°C/65– 70% RH and 75°C/15% RH] which was repeated 24 times. In general, a decrease in internal bond strength of all exposed specimens was observed but it was highest in the case of MUF-bonded joints. Furthermore, a significant decrease of the tensile strength of the wood adherend perpendicular to the grain in the tangential direction was determined after the cyclic climatic changes. The mechanical performance of the different adhesives in the bond line was tested by means of nanoindentation. Reduced values of elastic modulus, hardness, and total indentation were observed after climatic treatment, particularly for the rigid MUF adhesive, whereas the flexible adhesive EPI did not show such changes.
    Print ISSN: 0018-3830
    Electronic ISSN: 1437-434X
    Topics: Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Published by De Gruyter
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  • 10
    Publication Date: 2010-04-01
    Description: The tensile shear strength of veneer lap joints was characterised. The joints were produced with an Automated Bonding Evaluation System (ABES) using urea-formaldehyde (UF) as well as melamine-urea-formaldehyde (MUF) adhesive formulated for particleboard production. At a fixed heating temperature of 110°C, a systematic increase in bond strength was observed for both adhesives with increasing cure time. The absolute bond strength was significantly higher for MUF compared to UF. Nanoindentation experiments with the same specimens used for ABES revealed a very hard, stiff and brittle character of the UF resin, whereas the MUF proved significantly less hard and stiff, and less brit-tle. Wood cell walls in contact with adhesive, i.e., where adhesive penetration into the cell wall was assumed, showed significantly altered mechanical properties. Such cell walls were harder, stiffer and more brittle than unaffected reference cell walls. These effects were slightly more pronounced for UF than for MUF. Comparing UF and MUF, the micro-mechanical properties of cured adhesive and interphase cell walls confirm earlier observations that tougher adhesives can lead to higher macroscopic bond strength. In strong contrast to that, no obvious correlation was found between micromechanical properties and the strong cure time dependence of macroscopic bond strength.
    Print ISSN: 0018-3830
    Electronic ISSN: 1437-434X
    Topics: Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Published by De Gruyter
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