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(η6-Hexamethylbenzene)(mesidine)ditriflatoruthenium(II) (2000)

Feher, Frank J. ; Baldwin, Richard K. ; Ziller, Joseph W.

Oxford [u.a.] : International Union of Crystallography (IUCr)

Acta crystallographica 56 (2000), S. 633-634

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ISSN: 1600-5759

Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001

Topics: Chemistry and Pharmacology , Geosciences , Physics

Notes: The crystal structure of the title complex, (η6-hexamethylbenzene)bis(trifluoromethanesulfonato-O)(2,4,6-trimethylaniline-N)ruthenium(II), [Ru(CF3O3S)2(C12H18)(C9H13N)], is described. The complex has the classic three-legged piano-stool structure with a planar arene 1.667 Å from the metal, two monodentate O-bound trifluoromethanesulfonate ligands [Ru—O 2.169 (2) and 2.174 (2) Å] and one N-bound mesidine ligand [Ru—N 2.198 (2) Å]. The Ru—N distance is relatively long and the average Ru—O distance is relatively short when compared with previously characterized RuII complexes.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1107/S0108270100001001

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