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  • 1
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    International Union of Crystallography (IUC)
    Publication Date: 2012-12-09
    Description: Single crystals of the title compound, samarium aluminium germanium, were synthesized from the corresponding elements using molten Al metal as a solvent. The structure is isotypic with GdAl2.90Ge0.10, crystallizing in the hexagonal Ni3Sn structure type (space group P63/mmc), with two atoms in the asymmetric unit, namely Sm on Wyckoff site 2c and a statistical mixture of Al and Ge on Wyckoff site 6h. Structure refinement from single-crystal X-ray diffraction data result in the stoichiometry SmAl2.64 (4)Ge0.36 (4).
    Electronic ISSN: 1600-5368
    Topics: Chemistry and Pharmacology , Geosciences
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  • 2
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    Unknown
    International Union of Crystallography (IUC)
    Publication Date: 2012-12-09
    Description: Single crystals of the title compound, ytterbium hexamanganese hexastannide, were serendipitously synthesized from a reaction of elemental Yb, Mn and Bi in an Sn flux. The structure was determined by single-crystal X-ray diffraction to be an intermediate ordered state of the HfFe6Ge6 and YCo6Ge6 structures. This result confirms previous work on the structure of YbMn6Sn6 from X-ray and neutron powder diffraction data [Mazet et al. (1999). J. Magn. Magn. Mater. 204, 11–19], although the statistical distribution of Yb and Sn on the partially occupied sites is determined to be significantly different.
    Electronic ISSN: 1600-5368
    Topics: Chemistry and Pharmacology , Geosciences
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